WARNING: Personnel applying this standard should have practical experience in formal laboratory work. This section does not address all possible security issues. It is the user's responsibility to take appropriate safety and health measures and ensure compliance with the conditions stipulated in the relevant national laws and regulations. This part specifies the determination of silicon content in ferromanganese, manganese-silicon alloy, ferromanganese nitride, metallic manganese and electrolytic manganese by molybdenum blue photometric method, potassium fluorosilicate titration method and perchloric acid gravimetric method. This part is applicable to the determination of silicon content in ferromanganese, manganese-silicon alloy, ferromanganese nitride, metallic manganese and electrolytic metallic manganese. The determination range (mass fraction): 0.001% to 30.00%. Method 1: molybdenum blue photometry, suitable for the determination of silicon content in manganese metal and electrolytic metal manganese, the measurement range (mass fraction) is 0.001-0.60%; method 2: potassium fluorosilicate titration method, suitable for silicon content in manganese-silicon alloy Determination of content, measurement range (mass fraction) 12.00% ~ 30%; method three: perchloric acid gravimetric method, suitable for the determination of silicon content in ferromanganese, manganese-silicon alloy, ferromanganese nitride, metal manganese and electrolytic metal manganese , Determination range (mass fraction) 0.50% ~ 30.00%.
GB/T 5686.2-2008 Referenced Document
GB/T 4010 Ferroallys sampling and preparation of samples for chemical analysis*, 2015-09-11 Update
GB/T 5686.2-2008 history
2022GB/T 5686.2-2022 Ferromanganese, ferromanganese-silicon, nitrogen-bearing ferromanganese and manganese metal—Determination of silicon content—Molybdenum blue spectrophotometric method, silicon potassium fluoride titri
2008GB/T 5686.2-2008 Ferromanganese, ferromanganese-silicon, nitrogen-bearing ferromanganese and manganese metal. Determination of silicon content. Molybdenum blue photometric method, silicon potassium fluoride titrimetric method and perchloric acid dehydration gravimetric me
1985GB/T 5686.2-1985 Methods for chemical analysis of silicomanganese alloy--The gravimetric method for the determination of silicon content
GB/T 5686.2-2008 Ferromanganese, ferromanganese-silicon, nitrogen-bearing ferromanganese and manganese metal. Determination of silicon content. Molybdenum blue photometric method, silicon potassium fluoride titrimetric method and perchloric acid dehydration gravimetric me has been changed from GB/T 7730.2-2002 Ferromanganese and blast furnace ferromanganese--Determination of silicon content--Gravimetric method after perchloric acid dehydration.
GB/T 5686.2-2008 Ferromanganese, ferromanganese-silicon, nitrogen-bearing ferromanganese and manganese metal. Determination of silicon content. Molybdenum blue photometric method, silicon potassium fluoride titrimetric method and perchloric acid dehydration gravimetric me has been changed from GB/T 8654.3-1988 Methods for chemical analysis of manganese metal--The molybdenum blue photometric method for the determination of silicon content.