ASTM E2546-15
Standard Practice for Instrumented Indentation Testing

Standard No.

ASTM E2546-15

Release Date

2015

Published By

American Society for Testing and Materials (ASTM)

Status

Be replaced

Replace By

ASTM E2546-15(2023)

Latest

ASTM E2546-15(2023)

Scope

5.1 IIT Instruments are used to quantitatively measure various mechanical properties of thin coatings and other volumes of material when other traditional methods of determining material properties cannot be used due to the size or condition of the sample. This practice will establish the basic requirements for those instruments. It is intended that IIT based test methods will be able to refer to this practice for the basic requirements for force and displacement accuracy, reproducibility, verification, reporting, etc., that are necessary for obtaining meaningful test results.

5.2 IIT is not restricted to specific test forces, displacement ranges, or indenter types. This practice covers the requirements for a wide range of nano, micro, and macro (see ISO 14577-1) indentation testing applications. The various IIT instruments are required to adhere to the requirements of the practice within their specific design ranges.

1.1 This practice defines the basic steps of Instrumented Indentation Testing (IIT) and establishes the requirements, accuracies, and capabilities needed by an instrument to successfully perform the test and produce the data that can be used for the determination of indentation hardness and other material characteristics. IIT is a mechanical test that measures the response of a material to the imposed stress and strain of a shaped indenter by forcing the indenter into a material and monitoring the force on, and displacement of, the indenter as a function of time during the full loading-unloading test cycle.

1.2 The operational features of an IIT instrument, as well as requirements for Instrument Verification (Annex A1), Standardized Reference Blocks (Annex A2) and Indenter Requirements (Annex A3) are defined. This practice is not intended to be a complete purchase specification for an IIT instrument.

1.3 With the exception of the non-mandatory Appendix X4, this practice does not define the analysis necessary to determine material properties. That analysis is left for other test methods. Appendix X4 includes some basic analysis techniques to allow for the indirect performance verification of an IIT instrument by using test blocks.

1.4 Zero point determination, instrument compliance determination and the indirect determination of an indenter’s area function are important parts of the IIT process. The practice defines the requirements for these items and includes non-mandatory appendixes to help the user define them.

1.5 The use of deliberate lateral displacements is not included in this practice (that is, scratch testing).

1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appr......

ASTM E2546-15 Referenced Document

• ASTM E177 Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods
• ASTM E1875 Standard Test Method for Dynamic Young's Modulus, Shear Modulus, and Poisson's Ratio by Sonic Resonance
• ASTM E1876 Standard Test Method for Dynamic Young's Modulus, Shear Modulus, and Poisson's Ratio by Impulse Excitation of Vibration
• ASTM E3 Standard Practice for Preparation of Metallographic Specimens
• ASTM E384 Standard Test Method for Microindentation Hardness of Materials
• ASTM E691 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
• ASTM E74 Standard Practices for Calibration and Verification for Force-Measuring Instruments
• ASTM E92 Standard Test Method for Vickers Hardness of Metallic Materials
• ISO 376 Metallic materials - Calibration of force-proving instruments used for the verification of uniaxial testing machines

ASTM E2546-15 history

• 2023 ASTM E2546-15(2023) Standard Practice for Instrumented Indentation Testing
• 2015 ASTM E2546-15 Standard Practice for Instrumented Indentation Testing
• 2007 ASTM E2546-07e1 Standard Practice for Instrumented Indentation Testing
• 2007 ASTM E2546-07 Standard Practice for Instrumented Indentation Testing