ASTM D4065-20
Standard Practice for Plastics: Dynamic Mechanical Properties: Determination and Report of Procedures

Standard No.

ASTM D4065-20

Release Date

2020

Published By

American Society for Testing and Materials (ASTM)

Latest

ASTM D4065-20

Scope

1.1 This practice is for general use in gathering and reporting dynamic mechanical data. It incorporates laboratory practice for determining dynamic mechanical properties of plastic specimens subjected to various oscillatory deformations on a variety of instruments of the type commonly called dynamic mechanical analyzers or dynamic thermomechanical analyzers. 1.2 This practice is intended to provide means of determining the transition temperatures, elastic, and loss moduli of plastics over a range of temperatures, frequencies, or time, by free vibration and resonant or nonresonant forced vibration techniques. Plots of elastic and loss moduli are indicative of the viscoelastic characteristics of a plastic. These moduli are functions of temperature or frequency in plastics, and change rapidly at particular temperatures or frequencies. The regions of rapid moduli change are normally referred to as transition regions. 1.3 The practice is primarily useful when conducted over a range of temperatures from −140°C to polymer softening and is valid for frequencies from 0.01 to 1000 Hz. 1.4 This practice is intended for materials that have an elastic modulus in the range from 0.5 MPa to 100 GPa (73 psi to 1.5 × 107 psi). 1.5 Discrepancies in results are known to arise when obtained under differing experimental conditions. Without changing the observed data, reporting in full (as described in this practice) the conditions under which the data were obtained will enable apparent differences observed in another study to be reconciled. An assumption of this technique is that testing is conducted in the region of linear viscoelastic behavior. 1.6 Different modes of deformation, such as tensile, bending and shear, are used, as listed in the referenced test methods. 1.7 Test data obtained by this practice are relevant and appropriate for use in engineering design. 1.8 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only. 1.9 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Section 8. NOTE 1—This practice is equivalent to ISO 6721–1. 1.10 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM D4065-20 Referenced Document

• ASTM D4000 Standard Classification System for Specifying Plastic Materials*， 2023-03-15 Update
• ASTM D4092 Standard Terminology: Plastics: Dynamic Mechanical Properties
• ASTM D4440 Standard Test Method for Plastics: Dynamic Mechanical Properties: Melt Rheology
• ASTM D5023 Standard Test Method for Measuring the Dynamic Mechanical Properties: In Flexure (Three-Point Bending)
• ASTM D5024 Standard Test Method for Plastics: Dynamic Mechanical Properties: In Compression
• ASTM D5026 Standard Test Method for Plastics: Dynamic Mechanical Properties: In Tension
• ASTM D5279 Standard Test Method for Plastics: Dynamic Mechanical Properties: In Torsion
• ASTM D5418 Standard Test Method for Plastics: Dynamic Mechanical Properties: In Flexure (Dual Cantilever Beam)
• ASTM D618 Standard Practice for Conditioning Plastics for Testing*， 2021-07-15 Update
• ASTM E1867 Standard Test Method for Temperature Calibration of Dynamic Mechanical Analyzers
• ASTM E2254 Standard Test Method for Storage Modulus Calibration of Dynamic Mechanical Analyzers*， 2024-03-21 Update
• ASTM E2425 Standard Test Method for Loss Modulus Conformance of Dynamic Mechanical Analyzers*， 2021-10-01 Update
• ASTM E3142 Standard Test Method for Thermal Lag of Thermal Analysis Apparatus*， 2023-06-01 Update

ASTM D4065-20 history

• 2020 ASTM D4065-20 Standard Practice for Plastics: Dynamic Mechanical Properties: Determination and Report of Procedures
• 2012 ASTM D4065-12 Standard Practice for Plastics: Dynamic Mechanical Properties: Determination and Report of Procedures
• 2006 ASTM D4065-06 Standard Practice for Plastics: Dynamic Mechanical Properties: Determination and Report of Procedures
• 2001 ASTM D4065-01 Standard Practice for Plastics: Dynamic Mechanical Properties: Determination and Report of Procedures
• 1995 ASTM D4065-95 Standard Practice for Plastics: Dynamic Mechanical Properties: Determination and Report of Procedures