This standard specifies the principle, reagents and materials, instruments and equipment, sampling and preparation of samples, preparation work, experimental procedures, calculation results and precision for the determination of toluene insoluble content in coking products. This standard is applicable to the determination of toluene-insoluble content in coal tar pitch, modified pitch, impregnated pitch, coal pitch road construction oil, coal tar, wood preservative oil and coking feedstock oil for carbon black.