ASTM D7184-15
Standard Test Method for Ultra Low Nitrogen in Aromatic Hydrocarbons by Oxidative Combustion and Reduced Pressure Chemiluminescence Detection

Standard No.

ASTM D7184-15

Release Date

2015

Published By

American Society for Testing and Materials (ASTM)

Status

Be replaced

Replace By

ASTM D7184-15(2019)e1

Latest

ASTM D7184-20

Scope

5.1 This test method is useful to detect and quantify nitrogen-containing compounds at a concentration of 0.1 to 1.2 mg N/kg in light aromatic hydrocarbons used or produced in manufacturing process. These nitrogen-containing compounds are undesirable in finished aromatic products and may be used in setting specification for determining the total nitrogen content in aromatic hydrocarbons.

5.2 This test method requires the use of reduced pressure at the detector. Loss of vacuum or pressure fluctuations impact the sensitivity of the detector and the ability to determine nitrogen concentrations less than 1 mg N/kg.

1.1 This test method covers the determination of total nitrogen in aromatic hydrocarbons, such as benzene, toluene, and xylene.

1.2 This test method is applicable for samples containing nitrogen from 0.1 to 1.2 mg N/kg. For higher nitrogen concentrations refer to Test Method D4629. With careful analytical technique, this method can be used to successfully analyze concentrations below the current scope (see Appendix X1).

1.3 In determining the conformance of the test results using this method to applicable specifications; results shall be rounded off in accordance with the rounding-off method of Practice E29.

1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.5 This standard does not purport to address all of the safety concerns, if any associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 9.

ASTM D7184-15 Referenced Document

• ASTM D3437 Standard Practice for Sampling and Handling Liquid Cyclic Products
• ASTM D4629 Standard Test Method for Trace Nitrogen in Liquid Petroleum Hydrocarbons by Syringe/Inlet Oxidative Combustion and Chemiluminescence Detection
• ASTM D6809 Standard Guide for Quality Control and Quality Assurance Procedures for Aromatic Hydrocarbons and Related Materials
• ASTM E29 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
• ASTM E691 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method

ASTM D7184-15 history

• 2020 ASTM D7184-20 Standard Test Method for Ultra Low Nitrogen in Aromatic Hydrocarbons by Oxidative Combustion and Reduced Pressure Chemiluminescence Detection
• 2019 ASTM D7184-19 Standard Test Method for Ultra Low Nitrogen in Aromatic Hydrocarbons by Oxidative Combustion and Reduced Pressure Chemiluminescence Detection
• 2019 ASTM D7184-15(2019)e1 Standard Test Method for Ultra Low Nitrogen in Aromatic Hydrocarbons by Oxidative Combustion and Reduced Pressure Chemiluminescence Detection
• 2015 ASTM D7184-15 Standard Test Method for Ultra Low Nitrogen in Aromatic Hydrocarbons by Oxidative Combustion and Reduced Pressure Chemiluminescence Detection
• 2013 ASTM D7184-13 Standard Test Method for Ultra Low Nitrogen in Aromatic Hydrocarbons by Oxidative Combustion and Reduced Pressure Chemiluminescence Detection
• 2012 ASTM D7184-12 Standard Test Method for Ultra Low Nitrogen in Aromatic Hydrocarbons by Oxidative Combustion and Reduced Pressure Chemiluminescence Detection
• 2007 ASTM D7184-07 Standard Test Method for Ultra Low Nitrogen in Aromatic Hydrocarbons by Oxidative Combustion and Reduced Pressure Chemiluminescence