ASTM E1600-15
Standard Test Methods for Determination of Gold in Cyanide Solutions

Standard No.
ASTM E1600-15
Release Date
2015
Published By
American Society for Testing and Materials (ASTM)
Status
Replace By
ASTM E1600-23
Latest
ASTM E1600-23
Scope

4.1 In primary metallurgical processes for gold bearing ores, gold is extracted with an alkaline cyanide solution. Metallurgical accounting, process control, and ore evaluation procedures depend on accurate, precise, and prompt measurements of the gold concentrations.

4.2 These test methods are comparative referee methods for compliance with compositional specifications for metal concentration or to monitor processes. It is assumed that all who use these methods will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory under appropriate quality control practices such as those described in Guide E882, and that proper waste disposal procedures will be followed.

1.1 These test methods cover the determination of gold in ore processing cyanide solutions within the following ranges:

Method

Application Range,
μg/mL

Inductively Coupled Plasma Mass Spectrometry

0.001 to 0.500

Flame Atomic Absorption Spectrometry

0.300 to 10.0

Note 1: The lower limit for the Inductively Coupled Plasma Mass Spectrometry Method, 0.001 µg/mL, was set following the guidance of Practice E1601. The reproducibility Index, R, was calculated using the total standard deviation for the lowest concentration Youden pair solution.

1.1.1 These test methods may also be applied to cyanide leach solutions from metallurgical evaluation procedures.

1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.3 The test methods appear in the following order:

Method

Sections

Flame Atomic Absorption Spec......

ASTM E1600-15 Referenced Document

  • ASTM D1193 Standard Specification for Reagent Water
  • ASTM D1293 Standard Test Methods for pH of Water
  • ASTM D2777 Standard Practice for Determination of Precision and Bias of Applicable Methods of Committee D-19 on Water
  • ASTM D5673 Standard Test Method for Elements in Water by Inductively Coupled Plasma8212;Mass Spectrometry
  • ASTM D6888 Standard Test Method for Available Cyanides with Ligand Displacement and Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection
  • ASTM D7237 Standard Test Method for Free Cyanide and Aquatic Free Cyanide with Flow Injection Analysis (FIA) Utilizing Gas Diffusion Separation and Amperometric Detection
  • ASTM E1060 
  • ASTM E135 Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
  • ASTM E1601 Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
  • ASTM E173 
  • ASTM E29 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
  • ASTM E50 Standard Practice for Apparatus, Reagents, and safety Precautions for Chemical Analysis of Metals
  • ASTM E882 Standard Guide for Accountability and Quality Control in the Chemical Analysis Laboratory

ASTM E1600-15 history

  • 2023 ASTM E1600-23 Standard Test Methods for Determination of Gold in Cyanide Solutions
  • 2015 ASTM E1600-15 Standard Test Methods for Determination of Gold in Cyanide Solutions
  • 2013 ASTM E1600-13 Standard Test Method for Determination of Gold in Cyanide Solutions by Flame Atomic Absorption Spectrometry
  • 2007 ASTM E1600-07 Standard Test Method for Determination of Gold in Cyanide Solutions by Atomic Absorption Spectrometry
  • 2002 ASTM E1600-02 Standard Test Method for Determination of Gold in Cyanide Solutions by Atomic Absorption Spectrometry
  • 1996 ASTM E1600-96 Standard Test Method for Determination of Gold in Cyanide Solutions by Atomic Absorption Spectrometry
Standard Test Methods for  Determination of Gold in Cyanide Solutions



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