ASTM D2274-14
Standard Test Method for Oxidation Stability of Distillate Fuel Oil (Accelerated Method)

Standard No.

ASTM D2274-14

Release Date

2014

Published By

American Society for Testing and Materials (ASTM)

Status

Be replaced

Replace By

ASTM D2274-14(2019)

Latest

ASTM D2274-14(2019)

Scope

5.1 This test method provides a basis for the estimation of the oxidation stability of middle distillate fuels such as No. 2 fuel oil.

5.2 The test method may not provide a prediction of the quantity of insolubles that will form in field storage over any given period of time. The amount of insolubles formed in such field storage is subject to the specific conditions which are too variable for this test method to predict accurately.

5.3 Test Method D2274 yields results more rapidly than Test Method D4625, the 438201;°C bottle test. However, as a result of the significantly elevated temperature and the pure oxygen atmosphere, the nature and amount of insolubles may deviate to a greater extent than Test Method D4625 from those formed in field storage.

1.1 This test method covers the measurement of the inherent stability of middle distillate petroleum fuels under specified oxidizing conditions at 958201;°C.

Note 1: Fuels used in establishing the precision measures for this test method were described as gas oil, diesel fuel, No. 2 heating oil, and DFM, a Navy distillate fuel suitable for diesels, boilers, and gas turbines. (The term DFM is no longer used when referring to fuel meeting MIL-F-16884 requirements; rather it is called F76 as it conforms to NATO F76 requirements.) While the test method may be used for fuels outside the range of these fuels, the precision measures may not apply.

1.2 This test method is not applicable to fuels containing residual oil. This test method has not been validated for testing biodiesel, such as meeting Specification D6751 or blends of middle distillates and biodiesel, such as meeting Specification D7467, or both. Test Method D7462 has been determined to be suitable for testing B100 and all blends of middle distillates and biodiesel.

Note 2: No. 1 and No. 2 grades in Specifications D396 or D975 currently allow up to 58201;% biodiesel meeting Specification D6751. Samples containing biodiesel can result in partial dissolution or compromise of the membrane filter and give erroneous results.

1.3 The values given in SI units are to be regarded as the standard. The values in parentheses are for information only.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

ASTM D2274-14 Referenced Document

• ASTM D1193 Standard Specification for Reagent Water
• ASTM D381 Standard Test Method for Existent Gum in Fuels by Jet Evaporation
• ASTM D396 Standard Specification for Fuel Oils
• ASTM D4057 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
• ASTM D4177 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
• ASTM D4625 Standard Test Method for Distillate Fuel Storage Stability at 43176C (110176F)
• ASTM D6751 Standard Specification for Biodiesel Fuel Blendstock (B100) for Middle Distillate Fuels
• ASTM D7462 Standard Test Method for Oxidation Stability of Biodiesel (B100) and Blends of Biodiesel with Middle Distillate Petroleum Fuel (Accelerated Method)
• ASTM D7467 Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
• ASTM D943 Standard Test Method for Oxidation Characteristics of Inhibited Mineral Oils
• ASTM D975 Standard Specification for Diesel Fuel Oils

ASTM D2274-14 history

• 2019 ASTM D2274-14(2019) Standard Test Method for Oxidation Stability of Distillate Fuel Oil (Accelerated Method)
• 2014 ASTM D2274-14 Standard Test Method for Oxidation Stability of Distillate Fuel Oil (Accelerated Method)
• 2010 ASTM D2274-10 Standard Test Method for Oxidation Stability of Distillate Fuel Oil (Accelerated Method)
• 2003 ASTM D2274-03a(2008) Standard Test Method for Oxidation Stability of Distillate Fuel Oil (Accelerated Method)
• 2003 ASTM D2274-03a Standard Test Method for Oxidation Stability of Distillate Fuel Oil (Accelerated Method)
• 2003 ASTM D2274-03 Standard Test Method for Oxidation Stability of Distillate Fuel Oil (Accelerated Method)
• 2001 ASTM D2274-01a Standard Test Method for Oxidation Stability of Distillate Fuel Oil (Accelerated Method)
• 2001 ASTM D2274-01 Standard Test Method for Oxidation Stability of Distillate Fuel Oil (Accelerated Method)
• 1994 ASTM D2274-94(1999)e1 Standard Test Method for Oxidation Stability of Distillate Fuel Oil (Accelerated Method)