ASTM E968-02(2014) PDF

Scope: 5.1 Differential scanning calorimetry is used to determine the heat or enthalpy of transition. For this information to be meaningful in an absolute sense, heat flow calibration of the apparatus or comparison of the resulting data to that of a known standard is required.

5.2 This practice is useful in calibrating the heat flow axis of differential scanning calorimeters or quantitative differential thermal analyzers for subsequent use in the measurement of transition energies and specific heat capacities of unknowns.

1.1 This practice covers the heat flow calibration of differential scanning calorimeters over the temperature range from8201;−8201;130°C to 8201;+800°C.

1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.3 Computer or electronic based instruments, techniques or data manipulation equivalent to this practice may also be used.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of whoever uses this standard to consult and establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See also Section 7.

ASTM E968-02(2014) Referenced Document

ASTM E1142 Standard Terminology Relating to Thermophysical Properties
ASTM E473 Standard Terminology Relating to Thermal Analysis
ASTM E793 Standard Test Method for Enthalpies of Fusion and Crystallization by Differential Scanning Calorimetry
ASTM E967 Standard Practice for Temperature Calibration of Differential Scanning Calorimeters and Differential Thermal Analyzers

2002 ASTM E968-02(2014) Standard Practice for Heat Flow Calibration of Differential Scanning Calorimeters
2002 ASTM E968-02(2008) Standard Practice for Heat Flow Calibration of Differential Scanning Calorimeters
2002 ASTM E968-02 Standard Practice for Heat Flow Calibration of Differential Scanning Calorimeters
1999 ASTM E968-99 Standard Practice for Heat Flow Calibration of Differential Scanning Calorimeters