ASTM D5808-09a(2014)
Standard Test Method for Determining Chloride in Aromatic Hydrocarbons and Related Chemicals by Microcoulometry

Standard No.
ASTM D5808-09a(2014)
Release Date
2009
Published By
American Society for Testing and Materials (ASTM)
Status
Replace By
ASTM D5808-18
Latest
ASTM D5808-23
Scope

5.1 Organic as well as inorganic chlorine compounds can prove harmful to equipment and reactions in processes involving hydrocarbons.

5.2 Maximum chloride levels are often specified for process streams and for hydrocarbon products.

5.3 Organic chloride species are potentially damaging to refinery processes. Hydrochloric acid can be produced in hydrotreating or reforming reactors and this acid accumulates in condensing regions of the refinery.

1.1 This test method covers the organic chlorides in aromatic hydrocarbons, their derivatives, and related chemicals.

1.2 This test method is applicable to samples with chloride concentrations from 1 to 25 mg/kg.

1.3 This test method is preferred over Test Method D5194 for products, such as styrene, that are polymerized by the sodium biphenyl reagent.

1.4 In determining the conformance of the test results using this method to applicable specifications, results shall be rounded off in accordance with the rounding-off method of Practice E29.

1.5 Organic chloride values of samples containing inorganic chlorides will be biased high due to partial recovery of inorganic species during combustion. Interference from inorganic species can be reduced by water washing the sample before analysis. This does not apply to water soluble samples.

1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see 7.3 and Section 9.

ASTM D5808-09a(2014) Referenced Document

  • ASTM D1193 Standard Specification for Reagent Water
  • ASTM D1555M Standard Test Method for Calculation of Volume and Weight of Industrial Aromatic Hydrocarbons and Cyclohexane [Metric]
  • ASTM D3437 Standard Practice for Sampling and Handling Liquid Cyclic Products
  • ASTM D5194 Standard Test Method for Trace Chloride in Liquid Aromatic Hydrocarbons
  • ASTM D6809 Standard Guide for Quality Control and Quality Assurance Procedures for Aromatic Hydrocarbons and Related Materials
  • ASTM E29 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
  • ASTM E691 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method

ASTM D5808-09a(2014) history

  • 2023 ASTM D5808-23 Standard Test Method for Determining Chloride in Aromatic Hydrocarbons and Related Chemicals by Microcoulometry
  • 2020 ASTM D5808-20 Standard Test Method for Determining Chloride in Aromatic Hydrocarbons and Related Chemicals by Microcoulometry
  • 2018 ASTM D5808-18 Standard Test Method for Determining Chloride in Aromatic Hydrocarbons and Related Chemicals by Microcoulometry
  • 2009 ASTM D5808-09a(2014) Standard Test Method for Determining Chloride in Aromatic Hydrocarbons and Related Chemicals by Microcoulometry
  • 2009 ASTM D5808-09a Standard Test Method for Determining Chloride in Aromatic Hydrocarbons and Related Chemicals by Microcoulometry
  • 2009 ASTM D5808-09 Standard Test Method for Determining Chloride in Aromatic Hydrocarbons and Related Chemicals by Microcoulometry
  • 2003 ASTM D5808-03 Standard Test Method for Determining Organic Chloride in Aromatic Hydrocarbons and Related Chemicals by Microcoulometry
  • 1995 ASTM D5808-95 Standard Test Method for Determining Organic Chloride in Aromatic Hydrocarbons and Related Chemicals by Microcoulometry
Standard Test Method for Determining Chloride in Aromatic Hydrocarbons and Related Chemicals      by Microcoulometry



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