ASTM C1211-13
Standard Test Method for Flexural Strength of Advanced Ceramics at Elevated Temperatures

Standard No.

ASTM C1211-13

Release Date

2013

Published By

American Society for Testing and Materials (ASTM)

Status

Be replaced

Replace By

ASTM C1211-18

Latest

ASTM C1211-18(2023)

Scope

4.1 This test method may be used for material development, quality control, characterization, and design data generation purposes. This test method is intended to be used with ceramics whose flexural strength is ∼ 50 MPa (∼ 7 ksi) or greater.

4.2 The flexure stress is computed based on simple beam theory, with assumptions that the material is isotropic and homogeneous, the moduli of elasticity in tension and compression are identical, and the material is linearly elastic. The average grain size should be no greater than ¹/₅₀ of the beam thickness. The homogeneity and isotropy assumptions in the test method rule out the use of it for continuous fiber-reinforced composites for which Test Method C1341 is more appropriate.

4.3 The flexural strength of a group of test specimens is influenced by several parameters associated with the test procedure. Such factors include the testing rate, test environment, specimen size, specimen preparation, and test fixtures. Specimen and fixture sizes were chosen to provide a balance between the practical configurations and resulting errors as discussed in Test Method C1161, and Refs (1-3).⁴ Specific fixture and specimen configurations were designated in order to permit the ready comparison of data without the need for Weibull size scaling.

4.4 The flexural strength of a ceramic material is dependent on both its inherent resistance to fracture and the size and severity of flaws. Variations in these cause a natural scatter in test results for a sample of test specimens. Fractographic analysis of fracture surfaces, although beyond the scope of this test method, is highly recommended for all purposes, especially if the data will be used for design as discussed in Ref (4) and Practices C1322 and C1239.

4.5 This method determines the flexural strength at elevated temperature and ambient environmental conditions at a nominal, moderately fast testing rate. The flexural strength under these conditions may or may not necessarily be the inert flexural strength. Flexure strength at elevated temperature may be strongly dependent on testing rate, a consequence of creep, stress corrosion, or slow crack growth. If the purpose of the test is to measure the inert flexural strength, then extra precautions are required and faster testing rates may be necessary.

Note 6—Many ceramics are susceptible to either environmentally-assisted slow crack growth or thermally activated slow crack growth. Oxide ceramics, glasses, glass ceramics, and ceramics containing boundary phase glass are particularly susceptible to slow crack growth. Time dependent effects that are caused by environmental factors (e.g. water as humidity in air) may be minimized through the use of inert testing atmosphere such as dry nitrogen gas or vacuum. Alternatively, testing rates faster than specified in this standard may be used if the goal is to measure the inert strength. Thermally activated slow crack growth may occur at elevated temperature even in inert atmospheres. Testing rates faster than specified in this standard should be used if the goal is to measure the inert flexural strength. On the other hand, many ceramics such as boron carbide, silicon carbide, aluminum nitride and many silicon nitrides have no sensitivity to slow crack growth at room or moderately elevated temperatures a......

ASTM C1211-13 Referenced Document

• ASTM C1161 Standard Test Method for Flexural Strength of Advanced Ceramics at Ambient Temperature
• ASTM C1239 Standard Practice for Reporting Uniaxial Strength Data and Estimating Weibull Distribution Parameters for Advanced Ceramics
• ASTM C1322 Standard Practice for Fractography and Characterization of Fracture Origins in Advanced Ceramics
• ASTM C1341 Standard Test Method for Flexural Properties of Continuous Fiber-Reinforced Advanced Ceramic Composites
• ASTM C1368 Standard Test Method for Determination of Slow Crack Growth Parameters of Advanced Ceramics by Constant Stress Rate Strength Testing at Ambient Temperature
• ASTM C1465 Standard Test Method for Determination of Slow Crack Growth Parameters of Advanced Ceramics by Constant Stress-Rate Flexural Testing at Elevated Temperatures
• ASTM E220 Standard Test Method for Calibration of Thermocouples By Comparison Techniques
• ASTM E230 Standard Specification and Temperature-Electromotive Force (EMF) Tables for Standardized Thermocouples
• ASTM E4 Standard Practices for Force Verification of Testing Machines

ASTM C1211-13 history

• 2023 ASTM C1211-18(2023) Standard Test Method for Flexural Strength of Advanced Ceramics at Elevated Temperatures
• 2018 ASTM C1211-18 Standard Test Method for Flexural Strength of Advanced Ceramics at Elevated Temperatures
• 2013 ASTM C1211-13 Standard Test Method for Flexural Strength of Advanced Ceramics at Elevated Temperatures
• 2002 ASTM C1211-02(2008) Standard Test Method for Flexural Strength of Advanced Ceramics at Elevated Temperatures
• 2002 ASTM C1211-02 Standard Test Method for Flexural Strength of Advanced Ceramics at Elevated Temperatures
• 1998 ASTM C1211-98a Standard Test Method for Flexural Strength of Advanced Ceramics at Elevated Temperatures