ASTM D1266-13
Standard Test Method for Sulfur in Petroleum Products (Lamp Method)

Standard No.
ASTM D1266-13
Release Date
2013
Published By
American Society for Testing and Materials (ASTM)
Status
Replace By
ASTM D1266-18
Latest
ASTM D1266-18
Scope

4.1 This test method provides a means of monitoring the sulfur level of various petroleum products and additives. This knowledge can be used to predict performance, handling, or processing properties. In some cases the presence of sulfur components is beneficial to the product and monitoring the depletion of sulfur compounds provides useful information. In other cases the presence of sulfur compounds is detrimental to the processing or use of the product.

1.1 This test method covers the determination of total sulfur in liquid petroleum products in concentrations from 0.01 to 0.4 mass8201;% (Note 1). A special sulfate analysis procedure is described in Annex A1 that permits the determination of sulfur in concentrations as low as 5 mg/kg.

Note 1The comparable lamp method for the determination of sulfur in liquefied petroleum gas is described in Test Method D2784. For the determination of sulfur in heavier petroleum products that cannot be burned in a lamp, see the high pressure decomposition device method (Test Method D129) the quartz tube method (IP 63), or the high-temperature method (Test Method D1552).

1.2 The direct burning procedure (Section 9) is applicable to the analysis of such materials as gasoline, kerosine, naphtha, and other liquids that can be burned completely in a wick lamp. The blending procedure (Section 10) is applicable to the analysis of gas oils and distillate fuel oils, naphthenic acids, alkyl phenols, high sulfur content petroleum products, and many other materials that cannot be burned satisfactorily by the direct burning procedure.

1.3 Phosphorus compounds normally present in commercial gasoline do not interfere. A correction is given for the small amount of acid resulting from the combustion of the lead anti-knock fluids in gasolines. Appreciable concentrations of acid-forming or base-forming elements from other sources interfere when the titration procedure is employed since no correction is provided in these cases.

1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

ASTM D1266-13 Referenced Document

  • ASTM D1193 Standard Specification for Reagent Water
  • ASTM D129 Standard Test Method for Sulfur in Petroleum Products (General Bomb Method)
  • ASTM D1552 Standard Test Method for Sulfur in Petroleum Products (High-Temperature Method)
  • ASTM D2784 Standard Test Method for Sulfur in Liquefied Petroleum Gases (Oxy-Hydrogen Burner or Lamp)
  • ASTM D6299 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
  • ASTM D6300 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
  • ASTM D6792 Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
  • ASTM E11 Standard Specification for Wire Cloth and Sieves for Testing Purposes

ASTM D1266-13 history

  • 2018 ASTM D1266-18 Standard Test Method for Sulfur in Petroleum Products (Lamp Method)
  • 2013 ASTM D1266-13 Standard Test Method for Sulfur in Petroleum Products (Lamp Method)
  • 2007 ASTM D1266-07 Standard Test Method for Sulfur in Petroleum Products (Lamp Method)
  • 1998 ASTM D1266-98(2003)e1 Standard Test Method for Sulfur in Petroleum Products (Lamp Method)
  • 1998 ASTM D1266-98 Standard Test Method for Sulfur in Petroleum Products (Lamp Method)
  • 1995 ASTM D1266-91(1995) Standard Test Method for Sulfur in Petroleum Products (Lamp Method)
  • 1987 ASTM D1266-87 Standard Test Method for Sulfur in Petroleum Products (Lamp Method)
Standard Test Method for Sulfur in Petroleum Products (Lamp Method)



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