ASTM D7846-12
Standard Practice for Reporting Uniaxial Strength Data and Estimating Weibull Distribution Parameters for Advanced Graphites

Standard No.
ASTM D7846-12
Release Date
2012
Published By
American Society for Testing and Materials (ASTM)
Status
Replace By
ASTM D7846-16
Latest
ASTM D7846-21
Scope

5.1 Two- and three-parameter formulations exist for the Weibull distribution. This practice is restricted to the two-parameter formulation. An objective of this practice is to obtain point estimates of the unknown Weibull distribution parameters by using well-defined functions that incorporate the failure data. These functions are referred to as estimators. It is desirable that an estimator be consistent and efficient. In addition, the estimator should produce unique, unbiased estimates of the distribution parameters (6). Different types of estimators exist, including moment estimators, least-squares estimators, and maximum likelihood estimators. This practice details the use of maximum likelihood estimators.

5.2 Tensile and flexural specimens are the most commonly used test configurations for graphite. The observed strength values depend on specimen size and test geometry. Tensile and flexural test specimen failure data for a nearly isotropic graphite (7) is depicted in Fig. 1. Since the failure data for a graphite material can be dependent on the test specimen geometry, Weibull distribution parameter estimates (m^, σ^θ) shall be computed for a given specimen geometry.

Failure Strengths for Tensile Test Specimens (left)xA;and Flexural Test Specimens (right) for a Nearly Isotropic Graphite
FIG. 1 Failure Strengths for Tensile Test Specimens (left) and Flexural Test Specimens (right) for a Nearly Isotropic Graphite (7)

5.3 Many factors affect the estimates of the distribution parameters. The total number of test specimens plays a significant role. Initially, the uncertainty associated with parameter estimates decreases significantly as the number of test specimens increases. However, a point of diminishing returns is reached where the cost of performing additional strength tests may not be justified. This suggests a limit to the number of test specimens for determining Weibull parameters to obtain a desired level of confidence associated with a parameter estimate. The number of specimens needed depends on the precision required in the resulting parameter estimate or in the resulting confidence bounds. Details relating to the computation of confidence bounds (directly related to the precision of the estimate) are presented in 8.3 and 8.4.

1.1 This practice covers the reporting of uniaxial strength data for graphite and the estimation of probability distribution parameters for both censored and uncensored data. The failure strength of graphite materials is treated as a continuous random variable. Typically, a nu......

ASTM D7846-12 history

  • 2021 ASTM D7846-21 Standard Practice for Reporting Uniaxial Strength Data and Estimating Weibull Distribution Parameters for Advanced Graphites
  • 2016 ASTM D7846-16 Standard Practice for Reporting Uniaxial Strength Data and Estimating Weibull Distribution Parameters for Advanced Graphites
  • 2012 ASTM D7846-12 Standard Practice for Reporting Uniaxial Strength Data and Estimating Weibull Distribution Parameters for Advanced Graphites



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