1.1 These test methods cover procedures for the gravimetric analysis of the binder and hydrochloric Acid (HCL) insoluble particles in white and yellow thermoplastic traffic markings. The HCL insoluble particles can be retroreflective optics, such as glass beads or some other type of retroreflective optic, or non-retroreflective particles such as silica sand, or a combination of any two or more of these materials.
1.2 This standard does not address the physical separation and the individual quantification of each component when a mixture of two or more HCL insoluble materials is present. Rather it requires the user to visually evaluate the HCL insoluble material (obtained from following this test method) and report the types of materials present.
1.3 This standard does not purport to address the titanium dioxide or lead chromate pigment measurement (after ashing) which is detailed in Test Methods D1394 and D126.
1.4 This standard will attempt to address the interference of organic pigments with the binder results.
1.5 The analytical procedures appear in the following order:
1.6 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.7 This standard does not purport to address all of the safety concerns, if any......
ASTM D4797-12a Referenced Document
ASTM D126 Standard Test Methods for Analysis of Yellow, Orange, and Green Pigments Containing Lead Chromate and Chromium Oxide Green
ASTM D1394 Standard Test Methods for Chemical Analysis of White Titanium Pigments
ASTM D7307 Standard Practice for Sampling of Thermoplastic Pavement Marking Materials
ASTM D7308 Standard Practice for Sample Preparation of Thermoplastic Pavement Marking Materials
ASTM E177 Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods
ASTM E691 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D4797-12a history
2022ASTM D4797-17(2022) Standard Test Methods for Gravimetric Analysis of White and Yellow Thermoplastic Pavement Marking
2017ASTM D4797-17 Standard Test Methods for Gravimetric Analysis of White and Yellow Thermoplastic Pavement Marking
2012ASTM D4797-12a Standard Test Methods for Gravimetric Analysis of White and Yellow Thermoplastic Traffic Marking
2012ASTM D4797-12 Standard Test Methods for Gravimetric Analysis of White and Yellow Thermoplastic Traffic Marking
1988ASTM D4797-88(2007) Standard Test Methods for Chemical and Gravimetric Analysis of White and Yellow Thermoplastic Traffic Marking Containing Lead Chromate and Titanium Dioxide
2004ASTM D4797-88(2004) Standard Test Methods for Chemical and Gravimetric Analysis of White and Yellow Thermoplastic Traffic Marking Containing Lead Chromate and Titanium Dioxide
1988ASTM D4797-88(1998) Standard Test Methods for Chemical and Gravimetric Analysis of White and Yellow Thermoplastic Traffic Marking Containing Lead Chromate and Titanium Dioxide