ASTM D5394-02(2012)
Standard Specification for Reclaimed 1,1,1-Trichloroethane

Standard No.

ASTM D5394-02(2012)

Release Date

2002

Published By

American Society for Testing and Materials (ASTM)

Latest

ASTM D5394-02(2012)

Scope

1.1 This specification defines Type I (high quality reclaimed 1,1,1-trichloroethane, approximating MIL Specification), Type II (good quality reclaimed solvent), Type III (minimal acceptable reclaimed solvent).

1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For a specific hazards statement see Section 4.

1.3 1,1,1-trichloroethane also is known commercially as methyl chloroform.

TABLE 1 Properties, Type I

Property	Specification	Test Method
Appearance	Free of turbidity and suspended matter	D3741
1,1,1-trichloroethane, weight %, min	92	D6806
Nonvolatile residue, weight %, max	0.0040	D2109
Color, Pt-Co, max	25	D2108
Water, weight %, max	0.015	D3401
Acid acceptance as NaOH, weight %, min	0.20	D2942
Aluminum scratch test	PassesA	D2943
Acidity as HCl, weight %, max	0.001	D2989
Alkalinity as NaOH, weight %, max	0.020	D2106
Halide as Cl, weight %, max	0.0005	D2988

^A Distill 100 mL solvent, collect 50 mL distillate, and conduct scratch test on distillate and portion remaining in distillation flask.

TABLE 2 Properties, Type II

Proper...... ASTM D5394-02(2012) Referenced Document ASTM D2106 Standard Test Methods for Determination of Amine Acid Acceptance (Alkalinity) of Halogenated Organic Solvents*， 2024-04-19 Update ASTM D2108 Standard Test Method for Color of Halogenated Organic Solvents and Their Admixtures (Platinum-Cobalt Scale) ASTM D2109 Standard Test Methods for Nonvolatile Matter in Halogenated Organic Solvents and Their Admixtures ASTM D2942 Standard Test Method for Total Acid Acceptance of Halogenated Organic Solvents (Nonreflux Methods) ASTM D2943 Standard Test Method for Aluminum Scratch of 1,1,1-Trichloroethane to Determine Stability ASTM D2988 Standard Test Methods for Water-Soluble Halide Ion in Halogenated Organic Solvents and Their Admixtures ASTM D2989 Standard Test Method for Acidity-Alkalinity of Halogenated Organic Solvents and Their Admixtures ASTM D3401 Standard Test Methods for Water in Halogenated Organic Solvents and Their Admixtures ASTM D3741 Standard Test Methods for Appearance of Admixtures Containing Halogenated Organic Solvents*， 2024-04-19 Update ASTM D6806 Standard Practice for Analysis of Halogenated Organic Solvents and Their Admixtures by Gas Chromatography ASTM D5394-02(2012) history 2002 ASTM D5394-02(2012) Standard Specification for Reclaimed 1,1,1-Trichloroethane 2002 ASTM D5394-02(2007) Standard Specification for Reclaimed 1,1,1-Trichloroethane 2002 ASTM D5394-02 Standard Specification for Reclaimed 1,1,1-Trichloroethane 1997 ASTM D5394-97 Standard Specification for Reclaimed 1,1,1-Trichloroethane Copyright ©2024 All Rights Reserved