ASTM D4004-06(2012)
Standard Test Methods for Rubbermdash;Determination of Metal Content by Flame Atomic Absorption (AAS) Analysis

Standard No.
ASTM D4004-06(2012)
Release Date
2006
Published By
American Society for Testing and Materials (ASTM)
Status
Replace By
ASTM D4004-06(2017)
Latest
ASTM D4004-06(2021)
Scope

These test methods are suitable for process control, for product acceptance, and for research and development.

1.1 These test methods cover the determination of lead, zinc, copper, and manganese in raw rubber and rubber compounds, vulcanized or unvulcanized. The level at which the metals are present is taken into account by suitable adjustments of sample mass and dilution.

1.2 Certain compounding ingredients, present in the rubber sample will dictate which of the methods should be used. Refer to Section 3. Five methods of determination are as follows:

Sections
Method A8
Method B9
Method C10
Method D14-22
Method E23-31

1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

ASTM D4004-06(2012) Referenced Document

  • ASTM D1076 Standard Specification for Rubber-Concentrated, Ammonia Preserved, Creamed, and Centrifuged Natural Latex
  • ASTM D4483 Standard Practice for Determining Precision for Test Method Standards in the Rubber and Carbon Black Industries
  • ASTM E663 
  • ISO 1396 Vulcanized and unvulcanized compounded rubber — Determination of copper content — Zinc diethyldithiocarbamate photometric method
  • ISO 1655 Raw rubber and rubber latex — Determination of manganese content — Potassium periodate photometric method

ASTM D4004-06(2012) history

  • 2021 ASTM D4004-06(2021) Standard Test Methods for Rubber—Determination of Metal Content by Flame Atomic Absorption (AAS) Analysis
  • 2017 ASTM D4004-06(2017) Standard Test Methods for Rubber—Determination of Metal Content by Flame Atomic Absorption (AAS) Analysis
  • 2006 ASTM D4004-06(2012) Standard Test Methods for Rubbermdash;Determination of Metal Content by Flame Atomic Absorption (AAS) Analysis
  • 2006 ASTM D4004-06 Standard Test Methods for Rubber8212;Determination of Metal Content by Flame Atomic Absorption (AAS) Analysis
  • 1993 ASTM D4004-93(2002) Standard Test Methods for Rubber8212;Determination of Metal Content by Flame Atomic Absorption (AAS) Analysis
  • 1998 ASTM D4004-93(1998) Standard Test Methods for Rubber-Determination of Metal Content by Flame Atomic Absorption (AAS) Analysis
Standard Test Methods for  Rubbermdash;Determination of Metal Content by Flame Atomic Absorption (AAS) Analysis



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