ASTM D2549-02(2012)
Standard Test Method for Separation of Representative Aromatics and Nonaromatics Fractions of High-Boiling Oils by Elution Chromatography

Standard No.
ASTM D2549-02(2012)
Release Date
2002
Published By
American Society for Testing and Materials (ASTM)
Status
Replace By
ASTM D2549-02(2017)
Latest
ASTM D2549-23
Scope

The determination of compound types by mass spectrometry requires, in some instances, a preliminary separation of the petroleum sample into representative aromatics and nonaromatics fractions, as in Test Methods D2425, D2786, and D3239. This test method provides a suitable separation technique for this application.

1.1 This test method covers the separation and determination of representative aromatics and nonaromatics fractions from hydrocarbon mixtures that boil between 232 and 538°C (450 and 1000°F). Alternative procedures are provided for the separation of 2 g or 10 g of hydrocarbon mixture.

Note 18212;Some components may not be eluted from the chromatographic column for some types of samples under the conditions used in this method.

Note 28212;Test Method D2007 is an alternative method of separating high-boiling oils into polar compounds, aromatics, and saturates fractions.

1.2 An alternative procedure is provided to handle samples boiling below 232°C (450°F), but whose 5 % point is above 178°C (350°F) as determined by Test Method D2887. This procedure is given in Appendix X1.

1.3 The values stated in acceptable SI units are to be regarded as the standard. The values given in parentheses are provided for information purposes only.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and heal practices and determine the applicability of regulatory limitations prior to use.

ASTM D2549-02(2012) Referenced Document

  • ASTM D2007 Standard Test Method for Characteristic Groups in Rubber Extender and Processing Oils and Other Petroleum-Derived Oils by the Clay8212;Gel Absorption Chromatographic Method
  • ASTM D2425 Standard Test Method for Hydrocarbon Types in Middle Distillates by Mass Spectrometry
  • ASTM D2786 Standard Test Method for Hydrocarbon Types Analysis of Gas-Oil Saturates Fractions by High Ionizing Voltage Mass Spectrometry
  • ASTM D2887 Standard Test Method for Boiling Range Distribution of Petroleum Fractions by Gas Chromatography
  • ASTM D3239 Standard Test Method for Aromatic Types Analysis of Gas-Oil Aromatic Fractions by High Ionizing Voltage Mass Spectrometry

ASTM D2549-02(2012) history

  • 2023 ASTM D2549-23 Standard Test Method for Separation of Representative Aromatics and Nonaromatics Fractions of High-Boiling Oils by Elution Chromatography
  • 2017 ASTM D2549-02(2017) Standard Test Method for Separation of Representative Aromatics and Nonaromatics Fractions of High-Boiling Oils by Elution Chromatography
  • 2002 ASTM D2549-02(2012) Standard Test Method for Separation of Representative Aromatics and Nonaromatics Fractions of High-Boiling Oils by Elution Chromatography
  • 2002 ASTM D2549-02(2007) Standard Test Method for Separation of Representative Aromatics and Nonaromatics Fractions of High-Boiling Oils by Elution Chromatography
  • 2002 ASTM D2549-02 Standard Test Method for Separation of Representative Aromatics and Nonaromatics Fractions of High-Boiling Oils by Elution Chromatography
  • 1995 ASTM D2549-91(1995) Standard Test Method for Separation of Representative Aromatics and Nonaromatics Fractions of High-Boiling Oils by Elution Chromatography
Standard Test Method for Separation of Representative Aromatics and Nonaromatics Fractions of High-Boiling Oils by Elution Chromatography



Copyright ©2024 All Rights Reserved