ASTM D3454-11
Standard Test Method for Radium-226 in Water

Standard No.
ASTM D3454-11
Release Date
2011
Published By
American Society for Testing and Materials (ASTM)
Status
Replace By
ASTM D3454-18
Latest
ASTM D3454-21
Scope

The most prevalent of the five radium isotopes in ground water, having a half life greater than one day, are 226Ra and 228Ra. These two isotopes also present the greatest health risk compared to the other naturally occurring nuclides of equal concentrations if ingested via the water pathway.

Although primarily utilized on a water medium, this technique may be applicable for the measurement of the 226Ra content of any media once the medium has been completely decomposed and put into an aqueous solution.

The general methodology and basis of this technique are similar to the methodology 226Ra in Drinking Water (Radon Emanation Technique) as described in the document EPA-600//4-80-032.

1.1 This test method covers the measurement of soluble, suspended, and total radium-226 in water in concentrations above 3.7 × 103 Bq/L. This test method is not applicable to the measurement of other radium isotopes.

1.2 This test method may be used for quantitative measurements by calibrating with a radium-226 standard, or for relative measurements by comparing the measurements made with each other.

1.3 This test method does not meet the current requirements of Practice D2777.

1.4 The values stated in SI units are to be regarded as the standard. The inch-pound units given in parentheses are for information only.

1.5 Hydrofluoric acid (HF) is very hazardous and should be used in a well-ventilated hood. Wear rubber gloves, safety glasses or goggles, and a laboratory coat. Avoid breathing any HF fumes. Clean up all spills promptly and wash thoroughly after using HF.

1.6 This standard does not purport to address all of the other safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

ASTM D3454-11 Referenced Document

  • ASTM D1129 Standard Terminology Relating to Water
  • ASTM D1193 Standard Specification for Reagent Water
  • ASTM D2777 Standard Practice for Determination of Precision and Bias of Applicable Methods of Committee D-19 on Water
  • ASTM D3370 Standard Practices for Sampling Water from Closed Conduits
  • ASTM D3648 Standard Practices for the Measurement of Radioactivity
  • ASTM D3649 Standard Test Method for High-Resolution Gamma-Ray Spectrometry of Water
  • ASTM D3856 Standard Guide for Good Laboratory Practices in Laboratories Engaged in Sampling and Analysis of Water
  • ASTM D4448 Standard Guide for Sampling Ground-Water Monitoring Wells
  • ASTM D5847 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
  • ASTM D6001 Standard Guide for Direct-Push Water Sampling for Geoenvironmental Investigations
  • ASTM D7282 Standard Practice for Setup, Calibration, and Quality Control of Instruments Used for Radioactivity Measurements

ASTM D3454-11 history

  • 2021 ASTM D3454-21 Standard Test Method for Radium-226 in Water 
  • 2018 ASTM D3454-18 Standard Test Method for Radium-226 in Water 
  • 2011 ASTM D3454-11 Standard Test Method for Radium-226 in Water
  • 2005 ASTM D3454-05 Standard Test Method for Radium-226 in Water
  • 1997 ASTM D3454-97 Standard Test Method for Radium-226 in Water
Standard Test Method for  Radium-226 in Water



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