ASTM D6247-10
Standard Test Method for Determination of Elemental Content of Polyolefins by Wavelength Dispersive X-ray Fluorescence Spectrometry

Standard No.
ASTM D6247-10
Release Date
2010
Published By
American Society for Testing and Materials (ASTM)
Status
Replace By
ASTM D6247-18
Latest
ASTM D6247-18
Scope

Elemental analysis serves as a quality control measure for post-reactor studies, for additive levels in formulated resins, and for finished products. X-ray fluorescence spectrometry is an accurate and relatively fast method to determine mass fractions of multiple elements in polyethylene and polypropylene materials.

1.1 This test method covers a general procedure for the determination of elemental content in polyolefins by wavelength-dispersive X-ray fluorescence (WDXRF) spectrometry, in mass fraction ranges typical of those contributed by additives, catalysts, and reactor processes. The elements covered by this test method include fluorine, sodium, magnesium, aluminum, silicon, phosphorus, sulfur, calcium, titanium, chromium, and zinc in the composition ranges given in Table 1.

ASTM D6247-10 Referenced Document

  • ASTM C1118 Standard Guide for Selecting Components for Wavelength-Dispersive X-Ray Fluorescence (XRF) Systems
  • ASTM D4703 Standard Practice for Compression Molding Thermoplastic Materials into Test Specimens, Plaques, or Sheets
  • ASTM D883 Standard Terminology Relating to Plastics
  • ASTM E135 Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
  • ASTM E1361 Standard Guide for Correction of Interelement Effects in X-Ray Spectrometric Analysis
  • ASTM E1601 Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
  • ASTM E1621 Standard Guide for X-Ray Emission Spectrometric Analysis
  • ASTM E29 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications

ASTM D6247-10 history

  • 2018 ASTM D6247-18 Standard Test Method for Determination of Elemental Content of Polyolefins by Wavelength Dispersive X-ray Fluorescence Spectrometry
  • 2010 ASTM D6247-10 Standard Test Method for Determination of Elemental Content of Polyolefins by Wavelength Dispersive X-ray Fluorescence Spectrometry
  • 2004 ASTM D6247-98(2004) Standard Test Method for Analysis of Elemental Content in Polyolefins By X-Ray Fluorescence Spectrometry
  • 1998 ASTM D6247-98 Standard Test Method for Analysis of Elemental Content in Polyolefins By X-Ray Fluorescence Spectrometry
Standard Test Method for Determination of Elemental Content of Polyolefins by Wavelength Dispersive X-ray Fluorescence Spectrometry



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