ASTM D4275-02
Standard Test Method for Determination of Butylated Hydroxy Toluene (BHT) in Polymers of Ethylene and Ethylene-Vinyl Acetate (EVA) Copolymers By Gas Chromatography

Standard No.
ASTM D4275-02
Release Date
2002
Published By
American Society for Testing and Materials (ASTM)
Status
Replace By
ASTM D4275-09
Latest
ASTM D4275-17
Scope

Separation and identification of stabilizers used in the manufacture of polyethylene are necessary in order to correlate performance properties with polymer composition.

The BHT extraction procedure is made effective by the insolubility of the polymer sample in solvents generally used for gas chromatographic analysis.

1.1 This test method describes a procedure for the determination of butylated hydroxy toluene (BHT) (2,6-di-t-butyl-4-methyl-hydroxybenzene) in polymers of ethylene and ethylene-vinyl acetate (EVA) copolymers by solvent extraction followed by gas chromatographic analysis. Detection of the compound is achieved by flame ionization, and quantitative analysis is obtained by use of internal or external standards, as described in Practices E 260, E 355, and E 594.

1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 9.

Note 18212;There is no similar or equivalent ISO standard.

ASTM D4275-02 Referenced Document

  • ASTM D4968 Standard Practice for Annual Review of Test Methods and Specifications for Plastics
  • ASTM E260 Standard Practice for Packed Column Gas Chromatography
  • ASTM E355 Standard Practice for Gas Chromatography Terms and Relationships*2024-04-19 Update
  • ASTM E380 Standard Practice for Use of the Internation System of Units (SI) (the Modernized Metric System)
  • ASTM E594 Standard Practice for Testing Flame Ionization Detectors Used in Gas or Supercritical Fluid Chromatography
  • ASTM E691 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method

ASTM D4275-02 history

  • 2017 ASTM D4275-17 Standard Test Method for Determination of Butylated Hydroxy Toluene (BHT) in Polymers of Ethylene and Ethylene–Vinyl Acetate (EVA) Copolymers by Gas Chromatography
  • 2009 ASTM D4275-09 Standard Test Method for Determination of Butylated Hydroxy Toluene (BHT) in Polymers of Ethylene and Ethylenex2013;Vinyl Acetate (EVA) Copolymers By Gas Chromatography
  • 2002 ASTM D4275-02 Standard Test Method for Determination of Butylated Hydroxy Toluene (BHT) in Polymers of Ethylene and Ethylene-Vinyl Acetate (EVA) Copolymers By Gas Chromatography
  • 1996 ASTM D4275-96 Standard Test Method for Determination of Butylated Hydroxy Toluene (BHT) in Polymers of Ethylene and Ethylene-Vinyl Acetate (EVA) Copolymers By Gas Chromatography
Standard Test Method for Determination of Butylated Hydroxy Toluene (BHT) in Polymers of Ethylene and Ethylene-Vinyl Acetate (EVA) Copolymers By Gas Chromatography



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