This International Standard specifies a method for the simultaneous determination of the activity concentration
of various radionuclides emitting gamma rays with energies 40 keV < E < 2 MeV in water samples, by
gamma-ray spectrometry using germanium detectors with high energy resolution in combination with a
multichannel analyser.
NOTE The determination of the activity concentration of radionuclides emitting gamma rays with energy below
40 keV and above 2 MeV is also possible within the scope of this International Standard, provided both the calibration of
the measuring system and the shielding are adapted to this purpose.
This International Standard includes the procedures for energy calibration, determination of the energy
dependent sensitivity of the measuring system, the analysis of the spectra and the determination of the activity
concentration of the various radionuclides in the sample studied. It is only applicable to homogeneous
samples. Samples with activities typically between 1 Bq and 104 Bq can be measured as such, i.e. without
dilution or concentration of the sample or special (electronic) devices.
Depending on different factors, such as the energy of the gamma rays and the emission probability per
nuclear disintegration, the size and geometry of the sample and the detector, the shielding, the counting time
and other experimental parameters, the sample should be concentrated by evaporation when activities below
about 1 Bq have to be measured. Also, when the activity is considerably higher than 104 Bq, the sample
should be either diluted or an aliquot of the sample should be taken or the source to detector distance should
be increased, or a correction for pile-up effects should be applied.
ISO 10703:2007 Referenced Document
IEC 60973 Test procedures for germanium gamma-ray detectors
IEC 61151 Nuclear instrumentation; amplifiers and preamplifiers used with detectors of ionizing radiation; test procedures
IEC 61452 Nuclear instrumentation - Measurement of activity or emission rate of gamma- ray emitting radionuclides - Calibration and use of germanium-based spectrometers*, 2021-06-01 Update
ISO 31-9 Quantities and units — Part 9: Atomic and nuclear physics — Amendment 1
ISO 3696 Water for analytical laboratory use; Specification and test methods
ISO 5667-1 Water quality — Sampling — Part 1: Guidance on the design of sampling programmes and sampling techniques*, 2023-03-14 Update