BS 2782-3 Method 323D:1996 PDF

Scope: This part of ISO 6721 describes a torsional, non-resonance method for determining the components of the shear complex modulus G of solid polymers in the form of bars or rods at frequencies typically in the range 0,001 Hz to 100 Hz. The method is suitable for measuring dynamic storage moduli ranging from about 10 MPa, which is typical of values obtained for stiff rubbers, to values of about 10 GPa which are representative of fibre-reinforced plastics. Although materials with moduli less than 10 MPa may be stud-ied, more accurate measurements of their dynamic properties can be made using simple shear (see ISO 6721-6) or torsional deformations of thin layers between parallel plates. This method is particularly suited to the measurement of loss factors greater than 0,1 and may therefore be conveniently used to study the variation of dynamic properties with temperature and frequency through most of the glass-rubber relaxation region (see ISO 6721-1:1994, subclause 9.4). The availability of data determined over wide ranges of both frequency and temperature enable master plots to be derived, using frequency-temperature shift procedures, which display dynamic properties over an extended fre-quency range at different temperatures. Although loss factors below 0,1 may be more accu-rately determined using the torsion pendulum (see ISO 6721-2), the method described in this part of ISO 6721 enables a much wider and continuous fre-quency range to be covered.

BS 2782-3 Method 323D:1996 history

1996 BS 2782-3 Method 323D:1996 Methods of testing plastics. Mechanical properties. Torsional vibration. Non-resonance method