1.1 This test method describes the nondestructive assay of scrap or waste for plutonium content using passive thermalneutron coincidence counting. This test method provides rapid results and can be applied to a variety of carefully sorted materials in containers as large as several thousand liters in volume. The test method applies to measurements of 238 Pu, 240 Pu, and 242 Pu and has been used to assay items whose total plutonium content ranges from 10 mg to 6 kg (1).2
1.2 This test method requires knowledge of the relative abundances of the Pu isotopes to determine the total Pu mass (Test Method C1030).
1.3 This test method may not be applicable to the assay of scrap or waste containing other spontaneously fissioning nuclides.
1.3.1 This test method may give biased results for measurements of containers that include large amounts of hydrogenous materials.
1.3.2 The techniques described in this test method have been applied to materials other than scrap and waste (2, 3).
1.4 This test method assumes the use of shift-register-based coincidence technology (4).
1.5 Several other techniques that are often encountered in association with passive neutron coincidence counting exist. These include neutron multiplicity counting (5, 6, Test Method C1500), add-a-source analysis for matrix correction (7), flux probes also for matrix compensation, cosmic-ray rejection (8) to improve precision close to the detection limit, and alternative data collection electronics such as list mode data acquisition. Passive neutron coincidence counting may also be combined with certain active interrogation schemes as in Test Methods C1316 and C1493. Discussions of these established techniques are not included in this method.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
ASTM C1207-10(2018) Referenced Document
ASTM C1009 Standard Guide for Establishing a Quality Assurance Program for Analytical Chemistry Laboratories Within the Nuclear Industry
ASTM C1030 Standard Test Method for Determination of Plutonium Isotopic Composition by Gamma-Ray Spectrometry
ASTM C1068 Standard Guide for Qualification of Measurement Methods by a Laboratory Within the Nuclear Industry
ASTM C1128 Standard Guide for Preparation of Working Reference Materials for Use in the Analysis of Nuclear Fuel Cycle Materials
ASTM C1133/C1133M Standard Test Method for Nondestructive Assay of Special Nuclear Material in Low-Density Scrap and Waste by Segmented Passive Gamma-Ray Scanning
ASTM C1210 Standard Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within the Nuclear Industry
ASTM C1316 Standard Test Method for Nondestructive Assay of Nuclear Material in Scrap and Waste by Passive-Active Neutron Counting Using a 252 Cf Shuffler
ASTM C1458 Standard Test Method for Nondestructive Assay of Plutonium, Tritium and&x2009;241Am by Calorimetric Assay*, 2024-04-22 Update
ASTM C1490 Standard Guide for the Selection, Training and Qualification of Nondestructive Assay (NDA) Personnel*, 2023-01-01 Update
ASTM C1493 Standard Test Method for Non-Destructive Assay of Nuclear Material in Waste by Passive and Active Neutron Counting Using a Differential Die-Away System*, 2019-03-15 Update
ASTM C1500 Standard Test Method for Nondestructive Assay of Plutonium by Passive Neutron Multiplicity Counting*, 2024-04-22 Update
ASTM C1592/C1592M Standard Guide for Making Quality Nondestructive Assay Measurements*, 2021-06-01 Update
ASTM C1673 Standard Terminology of C26.10 Nondestructive Assay Methods*, 2024-04-22 Update
ASTM C986 Standard Guide for Developing Training Programs in the Nuclear Fuel Cycle
ASTM C1207-10(2018) history
2018ASTM C1207-10(2018) Standard Test Method for Nondestructive Assay of Plutonium in Scrap and Waste by Passive Neutron Coincidence Counting
2010ASTM C1207-10 Standard Test Method for Nondestructive Assay of Plutonium in Scrap and Waste by Passive Neutron Coincidence Counting
2003ASTM C1207-03 Standard Test Method for Nondestructive Assay of Plutonium in Scrap and Waste by Passive Neutron Coincidence Counting
1997ASTM C1207-97 Standard Test Method for Nondestructive Assay of Plutonium in Scrap and Waste by Passive Neutron Coincidence Counting