1.1 This test method applies to the determination of hydrogen in nuclear-grade uranium oxide powders and pellets to determine compliance with specifications. Gadolinium oxide (Gd2O3) and gadolinium oxide-uranium oxide powders and pellets may also be analyzed using this test method.
1.2 This standard describes a procedure for measuring the total hydrogen content of uranium oxides. The total hydrogen content results from absorbed water, water of crystallization, hydro-carbides and other hydrogenated compounds which may exist as fuel’s impurities.
1.3 This test method covers the determination of
0.05 to 200 µg of residual hydrogen.
1.4 This test method describes an electrode furnace carrier gas combustion system equipped with a thermal conductivity detector.
1.5 The preferred system of units is micrograms hydrogen per gram of sample (µg/g sample) or micrograms hydrogen per gram of uranium (µg/g U).
1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 9.
1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
ASTM C1457-18 Referenced Document
ASTM C753 Standard Specification for Nuclear-Grade, Sinterable Uranium Dioxide Powder
ASTM C776 Standard Specification for Sintered Uranium Dioxide Pellets for Light Water Reactors*, 2022-07-01 Update
ASTM C859 Standard Terminology Relating to Nuclear Materials
ASTM C888 Standard Specification for Nuclear-Grade Gadolinium Oxide (Gd2O3) Powder
ASTM C922 Standard Specification for Sintered Gadolinium Oxide-Uranium Dioxide Pellets for Light Water Reactors*, 2024-04-22 Update
ASTM C1457-18 history
2018ASTM C1457-18 Standard Test Method for Determination of Total Hydrogen Content of Uranium Oxide Powders and Pellets by Carrier Gas Extraction
2000ASTM C1457-00(2010)e1 Standard Test Method for the Determination of Total Hydrogen Content of Uranium Oxide Powders and Pellets by Carrier Gas Extraction
2000ASTM C1457-00(2005) Standard Test Method for the Determination of Total Hydrogen Content of Uranium Oxide Powders and Pellets by Carrier Gas Extraction
2000ASTM C1457-00 Standard Test Method for the Determination of Total Hydrogen Content of Uranium Oxide Powders and Pellets by Carrier Gas Extraction