This standard specifies the chemical analysis methods for refractory materials and ceramics composed of oxides. Samples are prepared by melting and casting glass slices, and X-ray fluorescence spectroscopy (hereinafter referred to as XRF) is used for determination. This standard applies to the material types listed in Chapter 3, and other refractory material types can be used for reference. Note 1: When the content of these elements in the sample exceeds a certain amount, such as tin, uranium, zinc and zinc, there will be difficulties in melting. In this case, refer to the corresponding literature. Note 2: For mass fractions greater than 9956 (dry basis ) components, these values can also be verified by direct measurement if all existing trace components and loss on ignition have been determined and obtained by subtraction.
GB/T 21114-2019 Referenced Document
GB/T 10325 "Shaped refractory products—Rule of acceptance,sampling and inspection"
GB/T 15000.7 Directives for the work of reference materials—Part 7:General requirements for the competence of reference material producters*, 2021-04-30 Update
GB/T 17617 Rule of sampling and inspection for refractory raw materials
GB/T 3286.8 Method for chemical analysis of limestone and dolomite.Part 8:The determination of loss on ignition.The gravimetric method
GB/T 4513.2 Monolithic (unshaped) refractory products—Part 2:Sampling for testing
GB/T 6005 Test sieves.Metal wire cloth,perforated metal plate and electroformed sheet.Nominal sizes of openings
GB/T 6900 Chemical analysis of alumina silica refractories
GB/T 21114-2019 history
2019GB/T 21114-2019 Refractories—Chemical analysis by X-ray fluorescence(XRF)—Fused cast-bead method
2008GB/T 21114-2007 X-ray Fluorescence Spectrochemical Analysis of Refractory Materials - Molten Glass Disk Method