1.1 This test method covers the determination of sulfur concentration in the range from
3.0 mg ⁄kg to 1000 mg ⁄kg in light liquid hydrocarbons and fuels with oxygenates boiling in the range from 26 °C to 274 °C (80 °F to 525 °F). NOTE 1—Preliminary data has shown that this test method is also applicable to the determination of sulfur in denatured fuel ethanol (Specification D4806), automotive spark ignition engine fuel (Specification D4814), Ed75–Ed85 (Specification D5798) or gasoline-oxygenate fuel blends with greater than 10 % ethanol. However, the precision for these materials has not been determined. Subcommittee D02.03 is undertaking activities to obtain precision statements for these materials.
1.2 Other materials falling within the distillation range specified in
1.1, but having sulfur concentrations above 1000 mg ⁄kg, may be tested using appropriate dilutions to bring them within the specified limit. In addition, sample types that may be outside the specified distillation range, such as diesels and biodiesels, may be analyzed by this test method.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. The preferred units are milligrams per kilogram (mg/kg).
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.For specific hazard statements, see Sections 7 – 9.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
ASTM D3120-08(2019) Referenced Document
ASTM D1193 Standard Specification for Reagent Water
ASTM D1298 Standard Test Method for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
ASTM D4052 Standard Test Method for Density and Relative Density of Liquids by Digital Density Meter
ASTM D4057 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM D4177 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
ASTM D4806 Standard Specification for Denatured Fuel Ethanol for Blending with Gasolines for Use as Automotive Spark-Ignition Engine Fuel
ASTM D4814 Standard Specification for Automotive Spark-Ignition Engine Fuel
ASTM D5798 Standard Specification for Fuel Ethanol (Ed75-Ed85) for Automotive Spark-Ignition Engines
ASTM D6299 Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance*, 2023-07-01 Update
ASTM D3120-08(2019) history
2019ASTM D3120-08(2019) Standard Test Method for Trace Quantities of Sulfur in Light Liquid Petroleum Hydrocarbons by Oxidative Microcoulometry
2008ASTM D3120-08(2014) Standard Test Method for Trace Quantities of Sulfur in Light Liquid Petroleum Hydrocarbons by Oxidative Microcoulometry
2008ASTM D3120-08 Standard Test Method for Trace Quantities of Sulfur in Light Liquid Petroleum Hydrocarbons by Oxidative Microcoulometry
2006ASTM D3120-06e1 Standard Test Method for Trace Quantities of Sulfur in Light Liquid Petroleum Hydrocarbons by Oxidative Microcoulometry
2006ASTM D3120-06 Standard Test Method for Trace Quantities of Sulfur in Light Liquid Petroleum Hydrocarbons by Oxidative Microcoulometry
2003ASTM D3120-03a Standard Test Method for Trace Quantities of Sulfur in Light Liquid Petroleum Hydrocarbons by Oxidative Microcoulometry
2003ASTM D3120-03 Standard Test Method for Trace Quantities of Sulfur in Light Liquid Petroleum Hydrocarbons by Oxidative Microcoulometry
1996ASTM D3120-96(2002)e1 Standard Test Method for Trace Quantities of Sulfur in Light Liquid Petroleum Hydrocarbons by Oxidative Microcoulometry
1996ASTM D3120-96 Standard Test Method for Trace Quantities of Sulfur in Light Liquid Petroleum Hydrocarbons by Oxidative Microcoulometry