ASTM D5241-92(2017) PDF

Scope: 1.1 This practice covers standard procedures for extraction of volatile and semi-volatile organic compounds from water using small volumes of solvents. 1.2 The compounds of interest must have a greater solubility in the organic solvent than the water phase. 1.3 Not all of the solvents that can be used in micro extraction are addressed in this practice. The applicability of a solvent to extract the compound(s) of interest must be demonstrated before use. 1.4 This practice provides sample extracts suitable for any technique amenable to solvent injection such as gas chromatography or high performance liquid chromatography (HPLC). 1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 9 1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM D5241-92(2017) Referenced Document

ASTM D1129 Standard Terminology Relating to Water
ASTM D1193 Standard Specification for Reagent Water
ASTM D3370 Standard Practices for Sampling Water from Closed Conduits
ASTM D3694 Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents
ASTM D3856 Standard Guide for Good Laboratory Practices in Laboratories Engaged in Sampling and Analysis of Water
ASTM D3973 Standard Test Method for Low-Molecular Weight Halogenated Hydrocarbons in Water
ASTM D4210 Standard Practice for Intralaboratory Quality Control Procedures and a Discussion on Reporting Low-Level Data
ASTM D4448 Standard Guide for Sampling Ground-Water Monitoring Wells
ASTM D5175 Standard Test Method for Organohalide Pesticides and Polychlorinated Biphenyls in Water by Microextraction and Gas Chromatography

2017 ASTM D5241-92(2017) Standard Practice for Micro-Extraction of Water for Analysis of Volatile and Semi-Volatile Organic Compounds in Water
2011 ASTM D5241-92(2011) Standard Practice for Micro-Extraction of Water for Analysis of Volatile and Semi-Volatile Organic Compounds in Water
1992 ASTM D5241-92(2004) Standard Practice for Micro-Extraction of Water for Analysis of Volatile and Semi-Volatile Organic Compounds in Water
1992 ASTM D5241-92(1998) Standard Practice for Micro-Extraction of Water for Analysis of Volatile and Semi-Volatile Organic Compounds in Water