ISO 12010:2019 PDF

Scope: This document specifies a method for the quantitative determination of the sum of short-chain polychlorinated n-alkanes also known as short-chain polychlorinated paraffins (SCCPs) in the carbon bond range n-C10 to n-C13 inclusive, in mixtures with chlorine mass fractions (“contents”) between 50 % and 67 %, including approximately 6000 of approximately 8000 congeners. This method is applicable to the determination of the sum of SCCPs in unfiltered surface water, ground water, drinking water and waste water using gas chromatography-mass spectrometry with electron capture negative ionization (GC-ECNI-MS). Depending on the capability of the GC-ECNI-MS instrument, the concentration range of the method is from 0,1 µg/l or lower to 10 µg/l. Depending on the waste water matrix, the lowest detectable concentration is estimated to be > 0,1 µg/l. The data of the interlaboratory trial concerning this method are given in Annex I.

ISO 12010:2019 Referenced Document

ISO 5667-1 Water quality — Sampling — Part 1: Guidance on the design of sampling programmes and sampling techniques*， 2023-03-14 Update
ISO 5667-3 Water quality*， 2024-02-01 Update
ISO 8466-1 Water quality — Calibration and evaluation of analytical methods — Part 1: Linear calibration function*， 2021-11-17 Update
ISO/TS 13530 Water quality - Guidance on analytical quality control for chemical and physicochemical water analysis

2019 ISO 12010:2019 Water quality — Determination of short-chain polychlorinated alkanes (SCCP) in water — Method using gas chromatography-mass spectrometry (GC-MS) and negative-ion chemical ionization (NCI)
2012 ISO 12010:2012 Water quality - Determination of short-chain polychlorinated alkanes (SCCPs) in water - Method using gas chromatography-mass spectrometry (GC-MS) and negative-ion chemical ionization (NCI)