ISO 22066:2020 Water quality — Determination of total cyanide — Method using segmented flow injection, in-line ultraviolet digestion analysis by gas diffusion and amperometric detection
International Organization for Standardization (ISO)
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ISO 22066:2020
Scope
This document specifies operationally defined methods for the determination of total cyanide in various types of water such as drinking water, ground water, surface water, wastewaters, metallurgical processing tailings reclaim solution, heap leach barren solution, mill slurry tailings filtrate and leaching solutions, with cyanide concentrations from 5 µg/l to 2000 mg/l expressed as cyanide ions in the undiluted sample. The range of application can be extended by reducing the sensitivity (Figure A.1.).
NOTE ISO 2080:2008, 3.105, defines free cyanide. The concentration of total cyanide as defined in necessarily all of the metal cyanide complexes present as determined by a specified analytical method.
In this method, six suitable mass concentration ranges from 5 µg/l to 50 µg/l, from 50 µg/l to 500 µg/l, from 0,5 mg/l to 5 mg/l, from 5 mg/l to 50 mg/l, from 50 mg/l to 500 mg/l and from 500 mg/l to 2000 mg/l are described.
ISO 22066:2020 Referenced Document
ISO 3696 Water for analytical laboratory use; Specification and test methods
ISO 8466-1 Water quality — Calibration and evaluation of analytical methods — Part 1: Linear calibration function*, 2021-11-17 Update
ISO 8466-2 Water quality - Calibration and evaluation of analytical methods and estimation of performance characteristics - Part 2: Calibration strategy for non-linear second-order calibration functions
ISO 22066:2020 history
2020ISO 22066:2020 Water quality — Determination of total cyanide — Method using segmented flow injection, in-line ultraviolet digestion analysis by gas diffusion and amperometric detection