This document specifies the principle, reagents, instruments, sampling and preparation of samples, test procedures, result calculation and precision for the determination of total sulfur content of coking benzene products. This document is applicable to the determination of the total sulfur content of coking benzene products, including coking benzene, coking toluene, coking xylene and intermediate products. The determination range of method 1 is 0.1 mg/kg~30 mg/kg, and the measurement range of method 2 is 0.1 mg/kg~100 mg/kg.