Use acetonitrile and water mixed solvents to extract by shaking, and use two derivatization reagents, methoxyamine hydrochloride and N,O-bis(trimethylsilyl)trifluoroacetamide, for derivatization, and then directly use gas chromatography hydrogen flame detection The instrument was used for detection, and phenyl-β-D-glucopyranoside was used as the internal standard, and the internal standard standard curve method was used for quantitative analysis.
T/GZTPA 0010-2021 history
2021T/GZTPA 0010-2021 Gas Chromatography Hydrogen Flame Ionization Method for Detection of Soluble Sugar in Guizhou Tea