ASTM D128-98(2019)
Standard Test Methods for Analysis of Lubricating Grease

Standard No.
ASTM D128-98(2019)
Release Date
2019
Published By
American Society for Testing and Materials (ASTM)
Latest
ASTM D128-98(2019)
Scope
1.1 These test methods for analysis cover greases of the conventional type, which consist essentially of petroleum oil and soap. The constituents that can be determined are soap, unsaponifiable matter (petroleum oil, and so forth), water, free alkalinity, free fatty acid, fat, glycerin, and insolubles. NOTE 1—Any of the test methods described herein are best used by an experienced grease analyst who may also be able to make appropriate adaptations of the techniques as occasion requires. 1.2 A supplementary test method is provided in Appendix X1. This test method is intended primarily for application to greases containing thickeners that are essentially insoluble in n-hexane, and to greases that cannot be analyzed by conventional methods because of the presence of such constituents as nonpetroleum fluids or nonsoap-type thickeners, or both. In some cases, these constituents can react with strong acid or alkaline solutions. 1.3 These test methods appear in the following order: Sections Ash Determination 7 – 11 Insolubles, Soap, Fat, Petroleum Oil, and Unsaponifiable Matter 12 – 20 Free Alkali and Free Acid 21 – 23 Water 24 Glycerin (Quantitative) 25 – 29 1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM D128-98(2019) Referenced Document

  • ASTM D1078 Standard Test Method for Distillation Range of Volatile Organic Liquids
  • ASTM D1193 Standard Specification for Reagent Water
  • ASTM D1353 Standard Test Method for Nonvolatile Matter in Volatile Solvents for Use in Paint, Varnish, Lacquer, and Related Products
  • ASTM D156 Standard Test Method for Saybolt Color of Petroleum Products (Saybolt Chromometer Method)
  • ASTM D217 Standard Test Methods for Cone Penetration of Lubricating Grease
  • ASTM D445 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (the Calculation of Dynamic Viscosity)
  • ASTM D473 Standard Test Method for Sediment in Crude Oils and Fuel Oils by the Extraction Method
  • ASTM D804 Terminology Relating to Naval Stores, Including Tall Oil and Related Products
  • ASTM D95 Standard Test Method for Water in Petroleum Products and Bituminous Materials by Distillation

ASTM D128-98(2019) history

Standard Test Methods for Analysis of Lubricating Grease


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