1.1 This test method covers equipment and methods for detecting gross defects and mechanical damage (including wear-through) in metallic coatings where the breaks in the coating penetrate down to a copper or copper alloy substrate.
1.2 This test method is suitable for coatings consisting of single or combined layers of any coating that does not significantly tarnish in an alkaline polysulfide solution. Examples are gold, nickel, tin, tin-lead, and palladium, or their alloys.
1.3 Recent reviews of porosity testing (which include those for gross defects) and testing methods can be found in literature.2,3 An ASTM guide to the selection of porosity and gross defect tests for electrodeposits and related metallic coatings is available as Guide B765. Other related porosity test standards are Test Methods B735, B741, B798, B799, and B809.
1.4 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
ASTM B866-95(2018) Referenced Document
ASTM B246 Standard Specification for Tinned Hard-Drawn and Medium-Hard-Drawn Copper Wire for Electrical Purposes*, 2021-10-01 Update
ASTM B374 Standard Terminology Relating to Electroplating
ASTM B488 Standard Specification for Electrodeposited Coatings of Gold for Engineering Uses
ASTM B542 Standard Terminology Relating to Electrical Contacts and Their Use*, 2019-11-01 Update
ASTM B545 Standard Specification for Electrodeposited Coatings of Tin
ASTM B605 Standard Specification for Electrodeposited Coatings of Tin-Nickel Alloy
ASTM B679 Standard Specification for Electrodeposited Coatings of Palladium for Engineering Use*, 2021-10-01 Update
ASTM B689 Standard Specification for Electroplated Engineering Nickel Coatings*, 2023-05-01 Update
ASTM B733 Standard Specification for Autocatalytic (Electroless) Nickel-Phosphorus Coatings on Metal
ASTM B735 Standard Test Method for Porosity in Gold Coatings on Metal Substrates by Nitric Acid Vapor
ASTM B741 Standard Test Method for Porosity In Gold Coatings On Metal Substrates By Paper Electrography
ASTM B765 Standard Guide for Selection of Porosity Tests for Electrodeposits and Related Metallic Coatings
ASTM B798 Standard Test Method for Porosity in Gold or Palladium Coatings on Metal Substrates by Gel-Bulk Electrography*, 2020-04-01 Update
ASTM B799 Standard Test Method for Porosity in Gold and Palladium Coatings by Sulfurous Acid/Sulfur-Dioxide Vapor*, 2020-04-01 Update
ASTM B809 Standard Test Method for Porosity in Metallic Coatings by Humid Sulfur Vapor ("Flowers-of-Sulfur")*, 2024-04-21 Update
ASTM B866-95(2018) history
2018ASTM B866-95(2018) Standard Test Method for Gross Defects and Mechanical Damage in Metallic Coatings by Polysulfide Immersion
1995ASTM B866-95(2013) Standard Test Method for Gross Defects and Mechanical Damage in Metallic Coatings by Polysulfide Immersion
1995ASTM B866-95(2008) Standard Test Method for Gross Defects and Mechanical Damage in Metallic Coatings by Polysulfide Immersion
1995ASTM B866-95(2003) Standard Test Method for Gross Defects and Mechanical Damage in Metallic Coatings by Polysulfide Immersion
1995ASTM B866-95 Standard Test Method for Gross Defects and Mechanical Damage in Metallic Coatings by Polysulfide Immersion