1.1 This test method covers the determination of alphaemitting uranium isotopes in soil. This test method describes one acceptable approach to the determination of uranium isotopes in soil.2
1.2 The test method is designed to analyze 10 g of soil. This test method may not be able to completely dissolve all forms of uranium in the soil matrix. Studies have indicated that the use of hydrofluoric acid to dissolve soil has resulted in lower values than results using total dissolution by fusion.
1.3 The lower limit of detection is dependent on count time, sample size, detector, background, and tracer yield. The chemical yield averaged 78 % in a single laboratory evaluation, and 66 % in an interlaboratory collaborative study.
1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 11.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
ASTM C1000-19 Referenced Document
ASTM C1163 Standard Test Method for Mounting Actinides for Alpha Spectrometry Using Neodymium Fluoride
ASTM C1284 Standard Practice for Electrodeposition of the Actinides for Alpha Spectrometry
ASTM C859 Standard Terminology Relating to Nuclear Materials
ASTM C998 Standard Practice for Sampling Surface Soil for Radionuclides
ASTM C999 Standard Practice for Soil Sample Preparation for the Determination of Radionuclides
ASTM D1193 Standard Specification for Reagent Water
ASTM D3084 Standard Practice for Alpha-Particle Spectrometry of Water
ASTM D3648 Standard Practices for the Measurement of Radioactivity
ASTM D7282 Standard Practice for Setup, Calibration, and Quality Control of Instruments Used for Radioactivity Measurements*, 2021-05-15 Update
ASTM C1000-19 history
2019ASTM C1000-19 Standard Test Method for Radiochemical Determination of Uranium Isotopes in Soil by Alpha Spectrometry
2011ASTM C1000-11 Standard Test Method for Radiochemical Determination of Uranium Isotopes in Soil by Alpha Spectrometry
2005ASTM C1000-05 Standard Test Method for Radiochemical Determination of Uranium Isotopes in Soil by Alpha Spectrometry
2000ASTM C1000-00 Standard Test Method for Radiochemical Determination of Uranium Isotopes in Soil by Alpha Spectrometry