ASTM E2927-16
Standard Test Method for Determination of Trace Elements in Soda-Lime Glass Samples Using Laser Ablation Inductively Coupled Plasma Mass Spectrometry for Forensic Comparisons

Standard No.
ASTM E2927-16
Release Date
2016
Published By
American Society for Testing and Materials (ASTM)
Status
Replace By
ASTM E2927-16e1
Latest
ASTM E2927-23
Scope
1.1 This test method covers a procedure for the quantitative elemental analysis of the following seventeen elements: lithium (Li), magnesium (Mg), aluminum (Al), potassium (K), calcium (Ca), iron (Fe), titanium (Ti), manganese (Mn), rubidium (Rb), strontium (Sr), zirconium (Zr), barium (Ba), lanthanum (La), cerium (Ce), neodymium (Nd), hafnium (Hf) and lead (Pb) through the use of Laser Ablation Inductively Coupled Plasma Mass Spectrometry (LA-ICP-MS) for the forensic comparison of glass fragments. The potential of these elements to provide the best discrimination among different sources of soda-lime glasses has been published elsewhere (1-5).2 Silicon (Si) is also monitored for use as a normalization standard. Additional elements may be added as needed, for example, tin (Sn) can be used to monitor the orientation of float glass fragments. 1.2 The method only consumes approximately 0.4 to 2 µg of glass per replicate and is suitable for the analysis of full thickness samples as well as irregularly shaped fragments as small as 0.1 mm by 0.4 mm in dimension. The concentrations of the elements listed above range from the low parts per million (µgg-1 ) to percent (%) levels in soda-lime-silicate glass, the most common type encountered in forensic cases. This standard method may be applied for the quantitative analysis of other glass types; however, some modifications in the reference standard glasses and the element menu may be required. 1.3 This standard does not replace knowledge, skill, ability, experience, education or training and should be used in conjunction with professional judgment. 1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. 1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. 1 This test method is under the jurisdiction of ASTM Committee E30 on Forensic Sciences and is the direct responsibility of Subcommittee E30.01 on Criminalistics. Current edition approved Dec. 1, 2016. Published April 2017. Originally approved in 2013. Last previous edition approved in 2013 as E2927 – 13. DOI: 10.1520/E2927-16. 2 The boldface numbers in parentheses refer to a list of references at the end of this standard. Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. 1 2. Referenced Documents

ASTM E2927-16 Referenced Document

  • ASTM C162 Standard Terminology of Glass and Glass Products
  • ASTM E177 Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods
  • ASTM E2330 Standard Test Method for Determination of Concentrations of Elements in Glass Samples Using Inductively Coupled Plasma Mass Spectrometry (ICP-MS) for Forensic Comparisons*2019-12-01 Update

ASTM E2927-16 history

  • 2023 ASTM E2927-23 Standard Test Method for Determination of Trace Elements in Soda-Lime Glass Samples Using Laser Ablation Inductively Coupled Plasma Mass Spectrometry for Forensic Comparisons
  • 2016 ASTM E2927-16e1 Standard Test Method for Determination of Trace Elements in Soda-Lime Glass Samples Using Laser Ablation Inductively Coupled Plasma Mass Spectrometry for Forensic Comparisons
  • 2016 ASTM E2927-16 Standard Test Method for Determination of Trace Elements in Soda-Lime Glass Samples Using Laser Ablation Inductively Coupled Plasma Mass Spectrometry for Forensic Comparisons
  • 2013 ASTM E2927-13 Standard Test Method for Determination of Trace Elements in Soda-Lime Glass Samples Using Laser Ablation Inductively Coupled Plasma Mass Spectrometry for Forensic Comparisons
Standard Test Method for Determination of Trace Elements in Soda-Lime Glass Samples Using Laser Ablation Inductively Coupled Plasma Mass Spectrometry for Forensic Comparisons



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