This standard specifies a gas chromatography-mass spectrometry method for the determination of six phthalate compounds in soil and sediments. This standard applies to dimethyl phthalate (DMP), diethyl phthalate (DEP), di-n-butyl phthalate (DBP), butyl benzyl phthalate in soil and sediments Determination of six phthalate ester compounds including BBP, di(2-ethylhexyl) phthalate (DEHP) and di-n-octyl phthalate (DNOP). Other phthalate compounds can also be measured by this method after verification. When the sampling volume is 10.0 g, the extraction volume is 20.0 ml, and the injection volume is 1.0 µl, the detection limit of this standard method for determining phthalate esters is 0.02 mg/kg ~ 0.05 mg/kg, and the lower detection limit is 0.08 mg /kg~0.20 mg/kg. See Appendix A for details.
HJ 1184-2021 Referenced Document
GB 17378.3 The specification for marine monitoring.Part3:Sample collection,storage and transportation
GB 17378.5 The specification for marine monitoring.Part 5:Sediment analysis
HJ 494 Water quality.Guidance on sampling techniques
HJ 613 Soil.Determination of dry matter and water content.Gravimetric method
HJ 834 Determination of Semivolatile Organic Compounds in Soil and Sediments by Gas Chromatography-Mass Spectrometry
HJ/T 166 Technical specification for soil environmental monitoring
HJ 1184-2021 history
2021HJ 1184-2021 Determination of 6 Phthalate Compounds in Soil and Sediment by Gas Chromatography-Mass Spectrometry