ASTM D5074-90(2022)
Standard Practice for Preparation of Natural-Matrix Sediment Reference Samples for Major and Trace Inorganic Constituents Analysis by Partial Extraction Procedures

Standard No.

ASTM D5074-90(2022)

Release Date

2022

Published By

American Society for Testing and Materials (ASTM)

Latest

ASTM D5074-90(2022)

Scope

1.1 This practice covers uniform procedures to develop, select, collect, prepare, and use oxidized, relatively unpolluted, aquatic natural-matrix bed-sediment reference samples for the collaborative testing of chemical methods of analysis for sediments and similar materials. Reference samples prepared using this practice are intended for use as natural sediments, analyzable for major, minor, and trace elements, and general physical/organic analyses only. The samples are not designed or tested for environmental pollutants such as trace organic compounds. 1.2 Few, if any, aquatic sediment reference materials have been certified, defined, or are even available for developing or evaluating partial and sequential extraction procedures. This practice describes factors and considerations in site selection, sample characteristics, collection, and subsequent raw sample treatment needed to prepare natural-matrix bed-material sediments for use as partial or sequential extraction procedure reference test samples. The user of this practice is cautioned that in light of the many variables that may affect natural materials, neither the list of factors included for evaluation nor preparation of natural-matrix reference samples should be considered as all inclusive. It is the user’s responsibility to ensure the validity and applicability of these practices for preparing specific-matrix samples appropriate for testing the constituents of interest and the operationally defined extraction procedures utilized. 1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM D5074-90(2022) Referenced Document

• ASTM D1129 Standard Terminology Relating to Water
• ASTM D3974 Standard Practices for Extraction of Trace Elements from Sediments
• ASTM D3975 Standard Practice for Development and Use (Preparation) of Samples for Collaborative Testing of Methods for Analysis of Sediments
• ASTM D3976 Standard Practice for Preparation of Sediment Samples for Chemical Analysis
• ASTM E691 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method

ASTM D5074-90(2022) history

• 2022 ASTM D5074-90(2022) Standard Practice for Preparation of Natural-Matrix Sediment Reference Samples for Major and Trace Inorganic Constituents Analysis by Partial Extraction Procedures
• 2019 ASTM D5074-90(2019)e1 Standard Practice for Preparation of Natural-Matrix Sediment Reference Samples for Major and Trace Inorganic Constituents Analysis by Partial Extraction Procedures
• 1990 ASTM D5074-90(2014) Standard Practice for Preparation of Natural-Matrix Sediment Reference Samples for Major and Trace Inorganic Constituents Analysis by Partial Extraction Procedures
• 1990 ASTM D5074-90(2008) Standard Practice for Preparation of Natural-Matrix Sediment Reference Samples for Major and Trace Inorganic Constituents Analysis by Partial Extraction Procedures
• 1990 ASTM D5074-90(2003) Standard Practice for Preparation of Natural-Matrix Sediment Reference Samples for Major and Trace Inorganic Constituents Analysis by Partial Extraction Procedures
• 1990 ASTM D5074-90(1999) Standard Practice for Preparation of Natural-Matrix Sediment Reference Samples for Major and Trace Inorganic Constituents Analysis by Partial Extraction Procedures