ASTM D6376-10(2017)e1 Standard Test Method for Determination of Trace Metals in Petroleum Coke by Wavelength Dispersive X-ray Fluorescence Spectroscopy
1.1 This test method covers the X-ray fluorescence spectrometric determination of total sulfur and trace metals in samples of raw or calcined petroleum coke. Elements determined using this test method are listed in Table 1.
1.2 Detection limits, sensitivity, and optimal element ranges will vary with matrices, spectrometer type, analyzing crystal, and other instrument conditions and parameters.
1.3 All analytes are determined as the element and reported as such. These include all elements listed in Table 1. This test method may be applicable to additional elements or concentration ranges if sufficient standards are available to produce proper calibration equations.
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
ASTM D6376-10(2017)e1 Referenced Document
ASTM D1552 Standard Test Method for Sulfur in Petroleum Products (High-Temperature Method)
ASTM D346 Standard Practice for Collection and Preparation of Coke Samples for Laboratory Analysis
ASTM D4057 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
ASTM D5056 Standard Test Method for Trace Metals in Petroleum Coke by Atomic Absorption
ASTM D5600 Standard Test Method for Trace Metals in Petroleum Coke by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
ASTM D6969 Standard Practice for Preparation of Calcined Petroleum Coke Samples for Analysis*, 2023-07-01 Update
ASTM D6970 Standard Practice for Collection of Calcined Petroleum Coke Samples for Analysis*, 2019-12-01 Update
ASTM E11 Standard Specification for Wire Cloth and Sieves for Testing Purposes
ASTM D6376-10(2017)e1 history
2017ASTM D6376-10(2017)e1 Standard Test Method for Determination of Trace Metals in Petroleum Coke by Wavelength Dispersive X-ray Fluorescence Spectroscopy
2010ASTM D6376-10 Standard Test Method for Determination of Trace Metals in Petroleum Coke by Wavelength Dispersive X-Ray Fluorescence Spectroscopy
2009ASTM D6376-09 Standard Test Method for Determination of Trace Metals in Petroleum Coke by Wavelength Dispersive X-Ray Fluorescence Spectroscopy
2006ASTM D6376-06 Standard Test Method for Determination of Trace Metals in Petroleum Coke by Wavelength Dispersive X-Ray Fluorescence Spectroscopy
2005ASTM D6376-05 Standard Test Method for Determination of Trace Metals in Petroleum Coke by Wavelength Dispersive X-Ray Fluorescence Spectroscopy
1999ASTM D6376-99 Standard Test Method for Determination of Trace Metals in Petroleum Coke by Wavelength Dispersive X-Ray Fluorescence Spectroscopy