This standard specifies a gas chromatography-mass spectrometry method for the determination of organochlorine pesticides in soil and sediments. This standard is applicable to the determination of 23 organochlorine pesticides in soil and sediments. The target substances include: α-666, hexachlorobenzene, β-666, γ-666, δ-666, 7 Chlorine, aldrin, heptachlor epoxide, α-chlordane, α-endosulfan, γ-chlordane, dieldrin, p,p'-DDE, endrin, β-endosulfan, p, p'-DDD, endosulfan sulfate, endrin aldehyde, o,p'-DDT, endrin ketone, p,p'-DDT, methoxychlor, mirex. After verification, other organochlorine pesticides can also be applied to this standard. When the sampling amount is 20.0g and the concentration volume is 1.0 ml, the full scan method is used for determination. The detection limit of the method is 0.02 mg/kg~0.09 mg/kg, and the lower limit of determination is 0.08 mg/kg~0.36 mg. /kg. See Appendix A for details.
HJ 835-2017 Referenced Document
GB 17378.3 The specification for marine monitoring.Part3:Sample collection,storage and transportation
GB 17378.5 The specification for marine monitoring.Part 5:Sediment analysis
HJ 613 Soil.Determination of dry matter and water content.Gravimetric method
HJ 783 soil and sediment—extraction of organic compounds—pressurized fluid extraction(pfe)
HJ/T 166 Technical specification for soil environmental monitoring
HJ 835-2017 history
2017HJ 835-2017 Soil and sediment – Determination of organochlorine pesticides– Gas chromatography/Mass spectrometry