ASTM D4541-22
Standard Test Method for Pull-Off Strength of Coatings Using Portable Adhesion Testers

Standard No.

ASTM D4541-22

Release Date

2022

Published By

American Society for Testing and Materials (ASTM)

Latest

ASTM D4541-22

Scope

1.1 This test method covers a procedure for evaluating the pull-off strength (commonly referred to as adhesion) of a coating system from metal substrates. Pull-off strength of coatings from concrete is described in Test Method D7234. This test offers two test protocols. Protocol 1 (test to fracture) determines the greatest perpendicular force (in tension) that a surface area can bear before a plug of material is detached. Protocol 2 (pass/fail) determines if the coated surface remains intact at a defined load criteria. Fracture will occur along the weakest plane within the system comprised of the test fixture, glue, coating system, and substrate, and will be exposed by the fracture surface. This test method maximizes tensile stress as compared to the shear stress applied by other methods, such as scratch or knife adhesion, and results may not be comparable. NOTE 1—The procedure in this standard was developed for metal substrates, but may be appropriate for other rigid substrates such as plastic and wood. Factors such as loading rate and flexibility of the substrate must be addressed by the user/specifier. NOTE 2—The procedure in this standard was developed for use on flat surfaces. The results could have greater variability with lower values and averages for surfaces other than flat. 1.2 Pull-off strength measurements depend upon material, instrumentation and test parameters. Results obtained by each test method may give different results. Results should only be assessed for each test method and not be compared with other instruments. There are five instrument types, identified as Test Methods B-F. It is imperative to identify the test method used when reporting results. NOTE 3—Method A, which appeared in previous versions of this standard, has been eliminated as its main use is for testing on concrete substrates (see Test Method D7234). 1.3 This test method describes a class of apparatus known as portable pull-off adhesion testers.2 They are capable of applying a concentric load and counter load to a single surface so that coatings can be tested even though only one side is accessible. Measurements are limited by the strength of adhesive bonds between the loading fixture and the specimen surface or the cohesive strengths of the glue, coating layers, and substrate. 1.4 This test can be destructive and spot repairs may be necessary. 1.5 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined. 1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM D4541-22 Referenced Document

• ASTM D2651 Standard Guide for Preparation of Metal Surfaces for Adhesive Bonding
• ASTM D3933 Standard Guide for Preparation of Aluminum Surfaces for Structural Adhesives Bonding (Phosphoric Acid Anodizing)
• ASTM D7234 Standard Test Method for Pull-Off Strength of Coatings on Concrete Using Portable Pull-Off Adhesion Testers*， 2022-12-01 Update
• ASTM E691 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method

ASTM D4541-22 history

• 2022 ASTM D4541-22 Standard Test Method for Pull-Off Strength of Coatings Using Portable Adhesion Testers
• 2017 ASTM D4541-17 Standard Test Method for Pull-Off Strength of Coatings Using Portable Adhesion Testers
• 2009 ASTM D4541-09e1 Standard Test Method for Pull-Off Strength of Coatings Using Portable Adhesion Testers
• 2009 ASTM D4541-09 Standard Test Method for Pull-Off Strength of Coatings Using Portable Adhesion Testers
• 2002 ASTM D4541-02 Standard Test Method for Pull-Off Strength of Coatings Using Portable Adhesion Testers
• 1995 ASTM D4541-95e1 Standard Test Method for Pull-Off Strength of Coatings Using Portable Adhesion Testers