ASTM D2892-20
Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)

Standard No.

ASTM D2892-20

Release Date

2020

Published By

American Society for Testing and Materials (ASTM)

Status

Be replaced

Replace By

ASTM D2892-23

Latest

ASTM D2892-23

Scope

1.1 This test method covers the procedure for the distillation of stabilized crude petroleum (see Note 1) to a final cut temperature of 400 °C Atmospheric Equivalent Temperature (AET). This test method employs a fractionating column having an efficiency of 14 to 18 theoretical plates operated at a reflux ratio of 5:1. Performance criteria for the necessary equipment is specified. Some typical examples of acceptable apparatus are presented in schematic form. This test method offers a compromise between efficiency and time in order to facilitate the comparison of distillation data between laboratories. NOTE 1—Defined as having a Reid vapor pressure less than 82.7 kPa (12 psi). 1.2 This test method details procedures for the production of a liquefied gas, distillate fractions, and residuum of standardized quality on which analytical data can be obtained, and the determination of yields of the above fractions by both mass and volume. From the preceding information, a graph of temperature versus mass % distilled can be produced. This distillation curve corresponds to a laboratory technique, which is defined at 15/5 (15 theoretical plate column, 5:1 reflux ratio) or TBP (true boiling point). 1.3 This test method can also be applied to any petroleum mixture except liquefied petroleum gases, very light naphthas, and fractions having initial boiling points above 400 °C. 1.4 This test method contains the following annexes and appendixes: 1.4.1 Annex A1—Test Method for the Determination of the Efficiency of a Distillation Column, 1.4.2 Annex A2—Test Method for the Determination of the Dynamic Holdup of a Distillation Column, 1.4.3 Annex A3—Test Method for the Determination of the Heat Loss in a Distillation Column (Static Conditions), 1.4.4 Annex A4—Test Method for the Verification of Temperature Sensor Location, 1.4.5 Annex A5—Test Method for Determination of the Temperature Response Time, 1.4.6 Annex A6—Practice for the Calibration of Sensors, 1.4.7 Annex A7—Test Method for the Verification of Reflux Dividing Valves, 1.4.8 Annex A8—Practice for Conversion of Observed Vapor Temperature to Atmospheric Equivalent Temperature (AET), 1.4.9 Appendix X1—Test Method for Dehydration of a Sample of Wet Crude Oil, and 1.4.10 Appendix X2—Practice for Performance Check. 1.5 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard. 1.6 WARNING—Mercury has been designated by many regulatory agencies as a hazardous substance that can cause serious medical issues. Mercury, or its vapor, has been demonstrated to be hazardous to health and corrosive to materials. Use Caution when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for additional information. The potential exists that selling mercury or mercury-containing products, or both, is prohibited by local or national law. Users must determine legality of sales in their location. 1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see Section 10. 1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. 1 This test method is under the jurisdiction of ASTM Committee D02 on Petroleum Products, Liquid Fuels, and Lubricants and is the direct responsibility of Subcommittee D02.08 on Volatility. Current edition approved June 1, 2020. Published June 2020. Originally approved in 1970. Last previous edition approved in 2019 as D2892 – 19. DOI: 10.1520/D2892-20. *A Summary of Changes section appears at the end of this standard Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee. 2. Referenced Documents

ASTM D2892-20 Referenced Document

• ASTM D1217 Standard Test Method for Density and Relative Density (Specific Gravity) of Liquids by Bingham Pycnometer
• ASTM D1298 Standard Test Method for Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method
• ASTM D2887 Standard Test Method for Boiling Range Distribution of Petroleum Fractions by Gas Chromatography
• ASTM D3710 Standard Test Method for Boiling Range Distribution of Gasoline and Gasoline Fractions by Gas Chromatography
• ASTM D4006 Standard Test Method for Water in Crude Oil by Distillation
• ASTM D4052 Standard Test Method for Density and Relative Density of Liquids by Digital Density Meter
• ASTM D4057 Standard Practice for Manual Sampling of Petroleum and Petroleum Products
• ASTM D4177 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products
• ASTM D5134 Standard Test Method for Detailed Analysis of Petroleum Naphthas through n-Nonane by Capillary Gas Chromatography
• ASTM D6300 Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
• ASTM D6729 Standard Test Method for Determination of Individual Components in Spark Ignition Engine Fuels by 100 Metre Capillary High Resolution Gas Chromatography
• ASTM D6730 Standard Test Method for Determination of Individual Components in Spark Ignition Engine Fuels by 100-Metre Capillary (with Precolumn) High-Resolution Gas Chromatography*， 2022-11-01 Update
• ASTM D6733 Standard Test Method for Determination of Individual Components in Spark Ignition Engine Fuels by 50-Metre Capillary High Resolution Gas Chromatography*， 2020-11-01 Update
• ASTM D941 

ASTM D2892-20 history

• 2023 ASTM D2892-23 Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
• 2020 ASTM D2892-20 Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
• 2019 ASTM D2892-19 Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
• 2018 ASTM D2892-18a Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
• 2018 ASTM D2892-18 Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
• 2017 ASTM D2892-17a Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
• 2017 ASTM D2892-17 Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
• 2016 ASTM D2892-16 Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
• 2015 ASTM D2892-15 Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
• 2013 ASTM D2892-13 Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
• 2011 ASTM D2892-11a Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
• 2011 ASTM D2892-11 Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
• 2010 ASTM D2892-10 Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
• 2005 ASTM D2892-05 Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
• 2003 ASTM D2892-03a Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
• 2003 ASTM D2892-03 Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
• 2001 ASTM D2892-01 Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
• 1999 ASTM D2892-99a Standard Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)