ASTM D6049-03(2017) Standard Test Method for Rubber Property—Measurement of the Viscous and Elastic Behavior of Unvulcanized Raw Rubbers and Rubber Compounds by Compression Between Parallel Plates
1.1 This test method is an adaptation of the German Standard DIN 53514, a further development of the former “Defo Test” (see Appendix X1).
1.2 This test method is capable of measuring and characterizing the rheological behavior (viscosity and elasticity) of unvulcanized raw rubbers and rubber compounds, relating to the macro structure of rubber polymers (average molecular weight, molecular weight distribution, long chain branching, and microand macro-gel).
1.3 The viscosity and elasticity of unvulcanized rubbers and rubber compounds are determined by subjecting cylindrical test pieces to a compression/recovery cycle. The dependency on shear rate at constant shear stress is evaluated and the material fatigue behavior is determined in repeat cycle testing.
1.4 The non-Newtonian viscous and elastic behavior of rubbers and rubber compounds can also be evaluated.
1.5 Statistical evaluation of the test data provides an indication of data variation, which may be employed as an estimate of the homogeneity of the material tested.
1.6 The values stated in SI units are to be regarded as the standard. The values in parentheses are for information only.
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
ASTM D6049-03(2017) Referenced Document
ASTM D297 Standard Test Methods for Rubber Products-Chemical Analysis
ASTM D4483 Standard Practice for Determining Precision for Test Method Standards in the Rubber and Carbon Black Industries
ASTM D6048 Standard Practice for Stress Relaxation Testing of Raw Rubber, Unvulcanized Rubber Compounds, and Thermoplastic Elastomers
ASTM D926 Standard Test Method for Rubber Property-Plasticity and Recovery (Parallel Plate Method)
ISO 5725 Precision of test methods; Determination of repeatability and reproducibility for a standard test method by inter-laboratory tests
ISO 7323 Rubber, raw and unvulcanized compounded - Determination of plasticity number and recovery number - Parallel-plate method
ASTM D6049-03(2017) history
2022ASTM D6049-03(2022) Standard Test Method for Rubber Property—Measurement of the Viscous and Elastic Behavior of Unvulcanized Raw Rubbers and Rubber Compounds by Compression Between Parallel Plates
2017ASTM D6049-03(2017) Standard Test Method for Rubber Property—Measurement of the Viscous and Elastic Behavior of Unvulcanized Raw Rubbers and Rubber Compounds by Compression Between Parallel Plates
2003ASTM D6049-03(2013) Standard Test Method for Rubber Propertymdash;Measurement of the Viscous and Elastic Behavior of Unvulcanized Raw Rubbers and Rubber Compounds by Compression Between Parallel Plates
2008ASTM D6049-03(2008) Standard Test Method for Rubber Property-Measurement of the Viscous and Elastic Behavior of Unvulcanized Raw Rubbers and Rubber Compounds by Compression Between Parallel Plates
2003ASTM D6049-03 Standard Test Method for Rubber Property8212;Measurement of the Viscous and Elastic Behavior of Unvulcanized Raw Rubbers and Rubber Compounds by Compression Between Parallel Plates
1996ASTM D6049-96 Standard Test Method for Rubber Property--Measurement of the Viscous and Elastic Behavior of Unvulcanized Raw Rubbers and Rubber Compounds by Compression Between Parallel Plates