1.1 This practice describes methods for the statistical analysis of laboratory results obtained from interlaboratory proficiency testing programs. As in accordance with Practice E1301, proficiency testing is the use of interlaboratory comparisons for the determination of laboratory testing or measurement performance. Conversely, collaborative study (or collaborative trial) is the use of interlaboratory comparisons for the determination of the precision of a test method, as covered by Practice E691.
1.1.1 Method A covers testing programs using single test results obtained by testing a single sample (each laboratory submits a single test result).
1.1.2 Method B covers testing programs using paired test results obtained by testing two samples (each laboratory submits one test result for each of the two samples). The two samples should be of the same material or two materials similar enough to have approximately the same degree of variation in test results.
1.2 Methods A and B are applicable to proficiency testing programs containing a minimum of 10 participating laboratories.
1.3 The methods provide direction for assessing and categorizing the performance of individual laboratories based on the relative likelihood of occurrence of their test results, and for determining estimates of testing variation associated with repeatability and reproducibility. Assumptions are that a majority of the participating laboratories execute the test method properly and that samples are of sufficient homogeneity that the testing results represent results obtained from each laboratory testing essentially the same material. Each laboratory receives the same instructions or protocol.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
ASTM E2489-16 Referenced Document
ASTM E1301 Standard Guide for Proficiency Testing by Interlaboratory Comparisons
ASTM E177 Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods
ASTM E178 Standard Practice for Dealing With Outlying Observations
ASTM E2586 Standard Practice for Calculating and Using Basic Statistics*, 2019-04-01 Update
ASTM E456 Standard Terminology for Relating to Quality and Statistics
ASTM E691 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E2489-16 history
2021ASTM E2489-21 Standard Practice for Statistical Analysis of One-Sample and Two-Sample Interlaboratory Proficiency Testing Programs
2016ASTM E2489-16 Standard Practice for Statistical Analysis of One-Sample and Two-Sample Interlaboratory Proficiency Testing Programs
2011ASTM E2489-11 Standard Practice for Statistical Analysis of One-Sample and Two-Sample Interlaboratory Proficiency Testing Programs
2006ASTM E2489-06e1 Standard Practice for Statistical Analysis of One-Sample and Two-Sample Interlaboratory Proficiency Testing Programs
2006ASTM E2489-06 Standard Practice for Statistical Analysis of One-Sample and Two-Sample Interlaboratory Proficiency Testing Programs