This document specifies the determination of urea content in diesel engine nitrogen oxide reducing agent urea aqueous solution (AUS32) - fully automatic Kjeldahl nitrogen analyzer method. This document is suitable for measuring the urea content in the nitrogen oxide reducing agent - urea aqueous solution (AUS32) used in the selective catalytic reduction system of diesel vehicles. When the urea content in the urea aqueous solution is between 30.0% and 35.0% (mass fraction), it can be used measured by this method.